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' 110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax :925-798-1622 444 <br /> hqp://WWW,mccampbell.com E-mail: main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project 1D: Geweke Date Sampled: 06/24/99 <br /> 4005 North Wilson Way Date Received: 06/28/99 <br />' Stockton, CA 95205 Client Contact: Kevin McKibben Date Extracted: 06/28-07/06/99 <br /> Client P.O: Date Analyzed: 06/28-07/06/99 <br />' EPA method 8260 Volatile Organics By GUMS <br /> Lab ID 14476 <br />' Client 1D MW-816-24-99 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone(°t ND<130 trans-1,3-Dichloropropene ND<50 <br />' Benzene ND<50 Ethylene dibromide ND<50 <br /> Bromobenzene ND<50 Ethylbenzene 600 <br /> Bromochloromethane ND<50 Hexachlorobutadiene ND<50 <br /> Bromodichloromethane ND<50 lodomethane ND<50 <br /> I Bromoform ND<50 Isopropylbenzene 160 <br /> Bromomethane ND<50 -Iso ro yl toluene ND<50 <br /> n-Butyl benzene 66 Methyl butyl ketoneND<50 <br /> sec-Butyl benzene ND<50 Methylene Chloride"' ND<50 <br />' ten-Butyl benzene ND<50 Methyl ethyl ketone(0 ND<50 <br /> Carbon Disulfide ND<50 Methyl isobutyl ketone�fl ND<50 <br /> Carbon Tetrachloride ND<50 Methyl tent-Butyl Ether(MTBE) --- <br /> Chlorobenzene ND<50 Naphthalene ND<300 <br /> Chloroethane ND<50 n-Prop l benzene 310 <br /> 2-Chloroethyl Vinyl Ether"' ND<50 Styrene"I ND<50 <br /> Chloroform ND<50 1,1,1,2-Tetrachloroethane ND<50 <br /> I Chloromethane ND<50 1,1,2,2-Tetrachloroethane ND<50 <br /> 2-Chlorotoluene ND<50 Tetrachloroethene ND<50 <br /> 4-Chlorotoluene ND<50 Toluene"" ND<50 <br /> Dibromochloromethane ND<50 1,2,3-Trichlorobenzene ND<50 <br /> 1,2-Dibromo-3-chloro ro ane ND<50 1,2,4-Trichlorobenzene ND<50 <br /> Dibromomethane ND<50 1,1,1-Trichloroethane ND<50 <br /> 1,2-Dichlorobenzene ND<50 1,1,2-Trichloroethane ND<50 <br /> 1,3-Dichlorobenzene ND<50 Trichloroethene ND<50 <br /> 1,4-Dichlorobenzene ND<50 Trichlorofluoromethane ND<50 <br /> Dichlorodifluoromethane ND<50 1,2,3-Trichloropropane ND<50 <br /> 1,I-Dichloroethane ND<50 1,2,4-Tri methylbenzene 1400 <br /> 1,2-Dichloroethane ND<50 1,3,5-Trimethylbenzene 380 <br />' I,1-Dichloroethene ND<50 Vinyl Acetate'"' ND<50 <br /> cis-1,2-Dichloroethene ND<50 Vinyl ChlorideND<50 <br /> trans-I 2-Dichloroethene ND<50 X lenes total t"' 990 <br /> 1,2-Dichloro ropane ND<50 Comments: <br /> 1 3-Dichloro ro ane ND<50 5urr2ate Recoveries <br /> 2,2-Dichloropropane ND<50 Dibromofluoromethane 108 <br /> 1,1-Dichloropropene ND<50 Toluene-d8 99 <br /> cis-1,3-Dichloro ro ene ND<50 4-Bromofluorobenzene 105 <br /> 'water and vapor samples are reported in ug/L„soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples I ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 uglkg;wipes 0.2ug/wipe <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene, (d) 2-hexanone; (e) dichloromethanc; (f) 2-butanone-, (g) 4-methyl-2- <br /> pentanone or isopropylacetonc; (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than —5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chlorcethene• o dime /benzenes. <br /> DHS Certification No. 1644 ( Edward Hamilton, Lab Director <br />