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1 110 2nd Avenue South,#137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> hU2://www.mcc4mpbell.com E-mail: main@mccampbell.com <br />' Advanced GeoEnvironmental Client Project ID: Geweke Date Sampled: 06/24/99 <br /> 4005 North Wilson Way Date Received: 06/28/99 <br />' Stockton, CA 95205 Client Contact: Kevin McKibben Date Extracted: 06/28-07106/99 <br /> Client P.O: Date Analyzed: 06/28-07/06/99 <br />' EPA method$260 Volatile Organics By GC/MS <br /> Lab ID 14477 <br />' Client 1D MW-9/6-24-99 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<I0 trans-1,3-Dichloropropene ND<10 <br />' Benzene ND<10 Ethylene dibromide ND<10 <br /> Bromobenzene ND<10 Ethylbenzene 220 <br /> Bromochloromethane ND<10 Hexachlorobutadiene ND<10 <br /> Bromodichloromethane ND<10 lodomethane ND<10 <br />' Bromoform ND<10 Isopropyl benzene 97 <br /> Bromomethane ND<10 -Isopropyl toluene ND<10 <br /> n-Butyl benzene 37 Methyl butyl ketone 1Q' ND<10 <br /> sec-Butyl benzene 22 Meth leve Ghloride16 ND<10 <br />' tert-Butyl benzene 17 Methyl ethyl ketone` ND<10 <br /> Carbon Disulfide ND<10 Methyl isobutyl ketone`g' ND<10 <br /> Carbon Tetrachloride ND<10 Methyl Cert-Butyl Ether(MTBE) _ <br /> Chlorobenzene ND<10 Naphthalene ND<100 <br /> Chloroethane ND<10 n-Propyl benzene 150 <br /> 2-Chloroeth I Vinyl Ether"' ND<10 Styrene°' ND<10 <br /> Chloroform ND<10 1,1,1,2-Teirach loroethane ND<]0 <br /> I Chloromethane ND<10 1,1.2,2-Tetrachloroethane ND<10 <br /> 2-Chlorotoluene ND<10 Tetrachloroethene ND<10 <br /> 4-Chlorotoluene ND<10 Toluene") ND<10 <br /> Dibromochloromethane ND<10 1,2,3-Tri chlorobenzene ND<10 <br /> 1,2-Dibromo-3-chloro ro ane ND<10 1,2,4-Trichiorobenzene ND<10 <br /> Dibromomethane ND<10 1,1,1-Trichioroethane ND<10 <br /> 1,2-Dichlorobenzene ND<10 1,1,2-Trichloroethane ND<10 <br /> 1,3-Dichlorobenzene ND<10 Trichloroethene ND<10 <br /> 1,4-Dichlorobenzene ND<10 Trichlorofluoromethane ND<10 <br /> Dichlorodifluoromethane ND<10 1,2,3-Trichloropropane ND<10 <br /> 1,1-Dichloroethane ND<10 1,2,4-Trimethylbenzene 670 <br /> 1,2-Dichloroethane 86 I,3,5-Trimethylbenzene 180 <br /> I I,1-Dichloroethene ND<10 Vinyl Acetate" ND<10 <br /> cis-1,2-Dichloroethene ND<10 Vinyl Chloride °} ND<10 <br /> trans-1,2-Dichloroethene ND<10 Xylenes,total 220 <br /> 1,2-Dichloro ropane ND<10 Comments: <br /> 1 3-Dichloro ro ane ND<10 Surrogate Reco%- ries <br /> 2,2-Dichloropropane ND<10 Dibromofluoromethane 112 <br /> l,1-Dichioropropene ND<10 Toluene-d8 100 <br /> cis-1,3-Dic1loro ro ene ND<10 4-Bromofluorobenzene 97 <br /> 'water.and vapor samples are reported in ug/L.,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated:water samples 1 ug/L;vapor samples 0.5 ug/L;solid and sludge samples 5 ug/kg;wipes 0.2ug/wipe <br /> ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetonc. (h) lighter than water immiscible sheen is present; (i) liquid sample that contains greater than —5 vol. % <br /> sediment; 0) sample diluted due to high organic content; (k) ethenylbenzene; (1) methylbenzene; (m) acetic acid ethenyl ester; (n) <br /> chloroethene; o dimethylbenzenes, <br /> DHS Certification No. 1644 Edward Hamilton, Lab Director <br /> I <br />