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Alpha Analytical, Inc. <br /> 255 Glendale Ave. • Suite 21 • Sparks, Nevada 89431-5778 <br /> (775)355-1044 • (775) 355-0406 FAX• 1-800-283-1183 <br /> Date: Work Order: <br /> 31-Oct-06 QC Summary Report 06102326 <br /> Method Blank Type MBLK Test Code: EPA Method SW8015B <br /> File ID: 06102506.D Batch ID: MS15S5932B Analysis Date: 10/25/2006 12:18 <br /> Sample ID: MBLK MS15S593213 Units : pg/Kg Run ID:MSD_15_061025B Prep Date: 10/25/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qua] <br /> TPH-P(GRO) ND 1000 <br /> Sum 1,2-Dichloroethane-d4 217 200 109 68 119 <br /> Surr:Toluene-d8 192 200 96 84 116 <br /> Surr:4-Bromofluorobenzene 184 200 92 72 118 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8015B <br /> File ID: 06102505.1) Batch ID: MS15S5932B Analysis Date: 10/25/2006 11:56 <br /> Sample ID: GLCS MS15S5932B Units : pg/Kg Run ID:MSD_15_061025B Prep Date: 10/25/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPH-P (GRO) 17600 2000 16000 110 60 153 <br /> Surr: 1,2-Dichloroethane-d4 450 400 112 68 119 <br /> Surr:Toluene-d8 369 400 92 84 116 <br /> Surr:4-Bromofluorobenzene 375 400 94 72 118 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8015B <br /> File ID: 06102518.13 Batch ID: MS15S5932B Analysis Date: 10/25%2006 16:48 <br /> Sample ID: 06102326-02AGS Units : pg/Kg Run ID:MSD_15_061025B Prep Date: 10/25/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPH-P(GRO) 14200 2000 16000 0 89 8 177 <br /> Surr: 1,2-Dichloroethane-d4 455 400 114 68 119 <br /> Surr:Toluene-d8 383 400 96 84 116 <br /> Surr:4-Bromofluorobenzene 382 400 95 72 118 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8015B <br /> File ID: 06102519.D Batch ID: MS15S5932B Analysis Date: 10/25/2006 17:11 <br /> Sample ID: 06102326-02AGSD Units : pg/Kg Run ID:MSD_15_061025B Prep Date: 10/25/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPH-P (GRO) 14600 2000 16000 0 91 8 177 14210 2.6(45) <br /> Surr: 1,2-Dichloroethane-d4 458 400 115 68 119 <br /> Surr:Toluene-d8 380 400 95 84 116 <br /> Surr:4-Bromofluorobenzene 376 400 94 72 118 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br /> Reported in micrograms per kilogram,per client request. <br />