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Alpha Analytical, Inc. <br /> 255 Glendale Ave. • Suite 21 • Sparks, Nevada 89431-5778 <br /> (775)355-1044 • (775) 355-0406 FAX• 1-800-283-1183 <br /> Date: QC Summary Report Work Order: <br /> 31-Oct-06 06102326 <br /> Method Blank Type MBLK Test Code: EPA Method SW8260B <br /> File ID: 06102506.D Batch ID: MS15S5932A Analysis Date: 10/25/2006 12:18 <br /> Sample ID: MBLK MS15S5932A Units : pg/Kg Run ID:MSD_15_061025B Prep Date: 10/25/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Tertiary Butyl Alcohol (TBA) ND 500 <br /> Methyl tert-butyl ether(MTBE) ND 5 <br /> Di-isopropyl Ether(DIPE) ND 20 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 20 <br /> Benzene ND 5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 20 <br /> Toluene ND 5 <br /> Ethylbenzene ND 5 <br /> m,p-Xylene ND 5 <br /> o-Xylene ND 5 <br /> Surr: 1,2-Dichloroethane-d4 217 200 109 68 119 <br /> Surr:Toluene-d8 192 200 96 84 116 <br /> Surr:4-Bromofluorobenzene 184 200 92 72 118 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8260B <br /> File ID: 06102504.D Batch ID: MS15S5932A Analysis Date: 10/25/2006 11:34 <br /> Sample ID: LCS MS15S5932A Units: pg/Kg Run ID:MSD_15_061025B Prep Date: 10/25/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 470 10 400 117 58 147 <br /> Toluene 404 10 400 101 58 148 <br /> Ethylbenzene 412 10 400 103 59 151 <br /> m,p-Xylene 442 10 400 110 60 155 <br /> o-Xylene 445 10 400 111 62 155 <br /> Surr: 1,2-Dichloroethane-d4 442 400 110 68 119 <br /> Surr:Toluene-d8 364 400 91 84 116 <br /> Surr:4-Bromofluorobenzene 374 400 94 72 118 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8260B <br /> File ID: 06102516.D Batch ID: MS15S5932A Analysis Date: 10/25/2006 16:03 <br /> Sample ID: 06102326-02AMS Units : pg/Kg Run ID:MSD_15_061025B Prep Date: 10/25/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 403 10 400 0 101 30 151 <br /> Toluene 350 10 400 0 88 25 159 <br /> Ethylbenzene 355 10 400 0 89 27 161 <br /> m,p-Xylene 377 10 400 0 94 22 170 <br /> o-Xylene 387 10 400 0 97 22 171 <br /> Surr: 1,2-Dichloroethane-d4 470 400 118 68 119 <br /> Surr:Toluene-d8 363 400 91 84 116 <br /> Surr:4-Bromofluorobenzene 376 400 94 72 118 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8260B <br /> File ID: 06102517.D Batch ID: MS15S5932A Analysis Date: 10/25/2006 16:26 <br /> Sample ID: 06102326-02AMSD Units : pg/Kg Run ID:MSD_15_061025B Prep Date: 10/25/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qua[ <br /> Benzene 416 10 400 0 104 30 151 403.4 3.0(37) <br /> Toluene 364 10 400 0 91 25 159 350.1 3.8(40) <br /> Ethylbenzene 366 10 400 0 92 27 161 355.2 3.1(39) <br /> m,p-Xylene 385 10 400 0 96 22 170 377 2.2(40) <br /> o-Xylene 396 10 400 0 99 22 171 387.3 2.2(41) <br /> Surr: 1,2-Dichloroethane-d4 462 400 116 68 119 <br /> Surr:Toluene-d8 371 400 93 84 116 <br /> Surr:4-Bromofluorobenzene 379 400 95 72 118 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br />