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Alpha Analytical, Inc. <br /> 255 Glendale Ave. • Suite 21 • Sparks, Nevada 89431-5778 <br /> (775) 355-1044 • (775) 355-0406 FAX • 1-800-283-1183 <br /> Date: QC SUmmary Report Work Order: <br /> 26-Oct-06 0610180 <br /> Method Blank Type MBLK Test Code: EPA Method SW8015B <br /> File ID: 06101940.11) Batch ID: MS15S5877B Analysis Date: 10/19/2006 23:17 <br /> Sample ID: MBLK MS15S5877B Units : pg/Kg Run ID:MSD_15_061019B Prep Date: 10/19/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPH-P (GRO) ND 1000 <br /> Surr: 1,2-Dichloroethane-d4 211 200 105 68 119 <br /> Surr:Toluene-d8 197 200 98 84 116 <br /> Surr:4-Bromofluorobenzene 186 200 93 72 118 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8015B <br /> File ID: 06101939.D Batch ID: MS15S5877B Analysis Date: 10/19/2006 22:54 <br /> Sample ID: GLCS MS15S5877B Units : pg/Kg Run ID:MSD_15_061019B Prep Date: 10/19/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPH-P (GRO) 15900 2000 16000 99 60 153 <br /> Surr: 1,2-Dichloroethane-d4 433 400 108 68 119 <br /> Surr:Toluene-d8 383 400 96 84 116 <br /> Surr:4-Bromofluorobenzene 379 400 95 72 118 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8015B <br /> File ID: 06101943.11) Batch ID: MS15S5877B Analysis Date: 10/20/2006 00:24 <br /> Sample ID: 06101805-01AGS Units : pg/Kg Run ID:MSD_15_061019B Prep Date: 10/20/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPH-P (GRO) 14500 2000 16000 0 91 8 177 <br /> Surr: 1,2-Dichloroethane-d4 422 400 106 68 119 <br /> Surr:Toluene-d8 386 400 97 84 116 <br /> Surr:4-Bromofluorobenzene 380 400 95 72 118 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8015B <br /> File ID: 06101944.11) Batch ID:MS15S5877B Analysis Date: 10/20/2006 00:47 <br /> Sample ID: 06101805-01AGSD Units : pg/Kg Run ID:MSD_15_061019B Prep Date: 10/20/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> TPH-P (GRO) 14000 2000 16000 0 87 8 177 14530 3.9(45) <br /> Surr: 1,2-Dichloroethane-d4 427 400 107 68 119 <br /> Surr:Toluene-d8 385 400 96 84 116 <br /> Surr: 4-Bromofluorobenzene 378 400 95 72 118 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br /> Reported in micrograms per kilogram,per client request. <br />