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Alpha Analytical, Inc. <br /> 255 Glendale Ave. • Suite 21 • Sparks, Nevada 89431-5778 <br /> (775) 355-1044 • (775) 355-0406 FAX• 1-800-283-1183 <br /> Date: f1C Summary Report Work Order: <br /> 16-Oct-06 V 06101805 <br /> Method Blank Type MBLK Test Code: EPA Method SW8260B <br /> File ID: 06101940.D Batch ID: MS15S5877A Analysis Date: 10/19/2006 23:17 <br /> Sample ID: MBLK MS15S5877A Units : pg/Kg Run ID:MSD_15_061019B Prep Date: 10/19/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Tertiary Butyl Alcohol(TBA) ND 500 <br /> Methyl tert-butyl ether(MTBE) ND 5 <br /> Di-isopropyl Ether(DIPE) ND 20 <br /> Ethyl Tertiary Butyl Ether(ETBE) ND 20 <br /> Benzene ND 5 <br /> Tertiary Amyl Methyl Ether(TAME) ND 20 <br /> Toluene ND 5 <br /> Ethylbenzene ND 5 <br /> m,p-Xylene ND 5 <br /> o-Xylene ND 5 <br /> Surr: 1,2-Dichloroethane-d4 211 200 105 68 119 <br /> Surr:Toluene-d8 197 200 98 84 116 <br /> Surr:4-Bromofluorobenzene 186 200 93 72 118 <br /> Laboratory Control Spike Type LCS Test Code: EPA Method SW8260B <br /> File ID: 06101938.13 Batch ID: MS15S5877A Analysis Date: 10/19/2006 22:32 <br /> Sample ID: LCS MS15S5877A Units : pg/Kg Run ID:MSD_15_061019B Prep Date: 10/19/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 458 10 400 115 58 147 <br /> Toluene 413 10 400 103 58 148 <br /> Ethylbenzene 411 10 400 103 59 151 <br /> m,p-Xylene 440 10 400 110 60 155 <br /> o-Xylene 451 10 400 113 62 155 <br /> Surr: 1,2-Dichloroethane-d4 437 400 109 68 119 <br /> Surr:Toluene-d8 376 400 94 84 116 <br /> Surr:4-Bromofluorobenzene 382 400 95 72 118 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8260B <br /> File ID: 06101941.D Batch ID: MS15S5877A Analysis Date: 10/19/2006 23:39 <br /> Sample ID: 06101805-01AMS Units : pg/Kg Run ID:MSD_15_061019B Prep Date: 10/19/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 398 10 400 0 99 30 151 <br /> Toluene 354 10 400 0 88 25 159 <br /> Ethylbenzene 355 10 400 0 89 27 161 <br /> m,p-Xylene 371 10 400 0 93 22 170 <br /> o-Xylene 388 10 400 0 97 22 171 <br /> Surr: 1,2-Dichloroethane-d4 436 400 109 68 119 <br /> Surr:Toluene-d8 372 400 93 84 116 <br /> Surr:4-Bromofluorobenzene 378 400 94 72 118 <br /> Sample Matrix Spike Duplicate Type MSD Test Code: EPA Method SW8260B <br /> File ID: 06101942.D Batch ID: MS15S5877A Analysis Date: 10/20/2006 00:02 <br /> Sample ID: 06101805-01AMSD Units : pg/Kg Run ID:MSD_15_061019B Prep Date: 10/20/2006 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit) Qual <br /> Benzene 417 10 400 0 104 30 151 398 4.7(37) <br /> Toluene 378 10 400 0 95 25 159 353.6 6.7(40) <br /> Ethylbenzene 382 10 400 0 95 27 161 355.2 7.2(39) <br /> m,p-Xylene 403 10 400 0 101 22 170 371.5 8.1(40) <br /> o-Xylene 411 10 400 0 103 22 171 387.7 5.8(41) <br /> Surr: 1,2-Dichloroethane-d4 432 400 108 68 119 <br /> Surr:Toluene-d8 375 400 94 84 116 <br /> Surr:4-Bromofluorobenzene 381 400 95 72 118 <br /> Comments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br />