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a 110 2nd Avenue South t1D7 Pacheco CA 94553 5560
<br /> McCampbell Analytical, Inc. Telephone 925-798 1620 Fax 925 798-1622
<br /> 24 Website www mccampbell corn E-mail matn@mccampbell com
<br /> Advanced GeoEnvironmental,Inc Client Project ID Cherokee Truck Stop Date Sampled 03/12/04
<br /> 837 Shaw Road Date Received 03/16/04
<br /> Client Contact Paul Dotson Date Extracted 03116/04-03/17/04
<br /> Stockton,CA 95215 Client P O Date Analyzed 03/16/04-03/17/04
<br /> Volatiles Organics by P&T and GC/MS(Banc Target List)*
<br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0403245
<br /> Lab ID 0403245-005B
<br /> Client ID UST 6
<br /> Matrix Water
<br /> Reportmg Rcportmg
<br /> Compound Concentration * DF L=t Compound Concentration* DF Lumt
<br /> Acetone ND 10 5 0 Acrolem(Propenal) ND 10 50
<br /> Acrylonitrtle ND 10 20 tert-Am 1 methyl ether TAME ND 10 05
<br /> Benzene ND 10 05 Bromobenzene ND 10 0 5
<br /> Bromochloromethane ND 10 05 Bromodichloromethane ND 10 0 5
<br /> Bromoform ND 10 0 5 Bromomethane ND 1 0 0 5
<br /> 2-Butanone(MEK) ND 10 10 t-Bu 1 alcohol BA) ND 1 0 5 0
<br /> n-But I benzene ND 10 0 5 sec-Butyl benzene ND 1 0 0 5
<br /> tert-But l benzene ND 10 05 Carbon Disulfide ND 1 0 0 5
<br /> Carbon Tetrachloride ND 10 05 Chlorobenzene ND 1 0 05
<br /> Chloroethane ND 10 05 2-Chloroeth i Vinyl Ether ND 1 0 1 0
<br /> Chloroform ND 1 0 0 5 Chloromethane ND 1 0 0 5
<br /> 2-Chlorotoluene ND 1 0 0 5 4-Chiorotoluene ND 1 0 0 5
<br /> Dibromechloromethane ND 1 0 0 5 1,2-Dibromo-3-chloro ro ane ND 1 0 0 5
<br /> 1,2-Dibromoethane(EDB) ND 1 0 05 Dibromomethane ND 1 0 0 5
<br /> 1,2-Dichlorobenzene ND 10 05 j 1,3-Dichlorobenzene ND 10 05
<br /> 1,4-Dichlorobenzene ND to 05 Dichlorodifluoromethane ND 1 0 0 5
<br /> 1,1-Dtchloroethene ND 10 0 5 1,2-Dtchloroethane 1,2-DCA 7 0 1 0 0 5
<br /> 1,1-Dtchloroethene ND 1 0 05 cis-1,2-Dtchloroethene ND 1 0 Os_
<br /> trans-1 2-Dtchloroethene ND 1 0 05 1,2-Dtchloro ro ane ND lo 0 5
<br /> 1,3-Dtchloropro ane ND 1 0 0 5 22-Dtchloro ro ane ND 1 0 0 5
<br /> 1,1-Dtchloropro ene ND 1 0 0 5 cis-1,3-Dtchloro roene ND 1 0 0 5
<br /> trans-l,3-Dichloropro ene ND 1 0 0 5 Diisopro yl ether DIPS ND 1 0 0 5
<br /> Eth lbenzene ND 1 0 0 5 Ethyl tert-but t ether(ETRE) ND 1 0 0 5
<br /> Hexachlorobutadiene ND 1 0 0 5 Hexachloroethane ND i 0 0 5
<br /> 2-Hexanone ND 10 0 5 fsopropylbenzene ND 1 0 0 5
<br /> 4-Isopropyl toluene ND 10 0 5 Meth l-t-but l ether MTBE 073 1 0 0 5
<br /> Methylene chloride 1 6 10 0 5 4-Meth 1-2- entanone(MD3K ND 10 0 5
<br /> Naphthalene ND 10 0 5 Nitrobenzene ND 1 0 10
<br /> n-Propyl benzene ND 10 0 5 St)Eene ND 1 0 0 5
<br /> 1,1,1,2-Tetrachloroethane ND 10 0 5 1,1,2,2-Tetrachloroethane ND 1 0 0 5
<br /> Tetrachloroethene ND 10 0 5 Toluene ND 1 0 0 5
<br /> 1,2,3-Tnchlorobenzene ND 1 to 0 5 1,2,4-Trichlorobenzene ND 1 0 05
<br /> 1,1,1-Tnchloroethane ND 10 0 5 1,1,2-Tnchloroethane ND 1 0 0 5
<br /> Trichloroethene ND to 0 5 Trichlorofluoromethane ND 1 0 0 5
<br /> 1,2,3-Tnchlororo ane ND 10 0 5 1,1,2-Tnchloro-1,2,2-tnfluoroethane ND 1 0 10
<br /> 1,2,4-Tnmeth lbenzene ND 10 0 5 1,3,5-Tnmeth lbenzene ND 1 0 0 5
<br /> Vinyl Chloride ND to 0 5 Xylenes ND 10 0 5
<br /> Surrogate Recoveries(%)
<br /> %SSI 104 °/aSS2 97 8
<br /> %SS3 103
<br /> Comments
<br /> "water and vapor samples and all TCLP&SPLP extracts are reported in gglL,soillsludgelsolid samples inµg/kg, wipe samples in lig/wipe,
<br /> product/otl/non-aqueous liquid samples in mg/L
<br /> ND means not detected above the reporting limit N/A means analyte not applicable to this analysis
<br /> surrogate diluted out of range or surrogate coelutes with another peak
<br /> h)lighter than water immiscible sheenlproduct is present,i)liquid sample that contains greater than--2 vol %sediment,j)sample diluted due to high
<br /> o anic content
<br /> DHS Certification No 1644 k—Angela Rydelius, Lab Manager
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