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a 110 2nd Avenue South,#D7 Pacheco,CA 94553-5560
<br /> McCampbell Analytical, Inc. Telephone 925-798-1620 Fax 925 798-1622
<br /> Website www mccampbell com E-mail rnainQmecampbell com
<br /> Advanced GeoEnvironmental, Inc Client Project tD Cherokee Truck Stop Date Sampled 03/12/04
<br /> 40 837 Shaw Road Date Received 03/16/04
<br /> Client Contact Paul Dotson Date Extracted 03/16/04-03/17/04
<br /> Stockton, CA 95215 Client P O Date Analyzed 03/16/04-03/17/04
<br /> Volatiles Organics by P&T and GC/MS(Basic Target List)*
<br /> Extraction Method SW5030B Aiialyttcal Method SW8260B Work Order 0403245
<br /> Lab ID 0403245-006B
<br /> Client ID UST 7
<br /> Matrix Water
<br /> Reporting
<br /> Compound Concentration ' DF ReL°mrtI s Compound Concentration* DF I.=
<br /> Acetone ND 10 50 Acrolem(Propenal) ND 1 0 50
<br /> Acrylonitrile ND 10 20 tert-Am l methyl ether(TAME) ND 10 05
<br /> Benzene ND 10 0 5 Bromobenzene ND 1 0 0 5
<br /> Bromochloromethane ND 10 0 5 Bromodichloromethane ND 1 0 0 5
<br /> Bromoform ND 10 0 5 Bromomethane ND 1 0 0 5
<br /> 2-Butanone(MEK) ND 10 1-0 t-Bu 1 alcohol TBA NO 1 0 5 0
<br /> n-But I benzene ND 10 0 5 sec-But)d benzene ND 1 0 0 5
<br /> tert-Butyj benzene ND 10 0 5 Carbon Disulfide ND 1 0 0 5
<br /> Carbon Tetrachloride ND 10 0 5 Chlorobenzene ND 1 0 0 5
<br /> Chloroethane ND 10 0 5 2-Chloroeth l Vinyl Ether ND 1 0 1 0
<br /> Chloroform ND 1 0 0 5 Chloromethane ND 1 0 0 5
<br /> 2-Chlorotoluene ND 1 0 0 5 4-Chlorotoluene ND 1 0 0 5
<br /> Dibromochloromethane ND l 0 0 5 1,2-Dibromo-3-chloro ro ane ND 1 0 0 5
<br /> 1,2-Dibromoethane(EDB) ND 1 0 0 5 Dihromomethane ND 1 0 0 5
<br /> 1,2-Dichlorobenzene ND 1 0 0 5 1,3-Dichlorobenzene ND 1 0 0 5
<br /> 1 4-Dichlorobenzene ND 10 0 5 Dichlorodifluoromethane ND 1 0 0 5
<br /> ],I-Dlchloroethane ND 1 0 0 5 1,2-Dichloroethane(1,2-DCA ND 1 0 0 5
<br /> 1,1-DiLhloroethene ND 10 0 5 cis-1,2-Dit.hloroethene ND 1 0 0 5
<br /> trans-l,2-Dichloroethene ND 10 0 5 1,2-Dichloro ro ane ND 1 0 0 5
<br /> 1 3-Dichlororo ane ND 1 0 0 5 2,2-Dichloro ro ane ND 1 0 0 5
<br /> 1 I-Dtchloro ro ene ND 1 0 0 5 cis-1,3-Dichloro ri7 ene ND 1 0 0 5
<br /> trans-l,3-Dichloro ro ene ND 10 0 5 Diiso ro 1 ether DIPS ND 1 0 0 5
<br /> Eth lbenzene ND 1 0 0 5 Ethyl tert-butyl ether ETRE) ND 1 0 0 5
<br /> Hexachlorobutadiene ND 1 0 0 5 Hexachloroethane ND 1 0 0 5
<br /> 2-Hexanone ND 1 0 0 5 Iso rop lbenzene ND 1 0 0 5
<br /> 4-lsopLopyLtoluene ND 1 0 0 5 Meth 1-t-butyl ether MTBE ND 1 0 0 5
<br /> Methylene chlonde 1 8 1 0 0 5 4-Meth 1-2- entanone(MIRK) ND 1 0 0 5
<br /> Naphthalene ND 10 0 5 Nitrobenzene ND 1 0 10
<br /> n-Propyl benzene ND 1 0 0 5 Stymne ND 1 0 0 5
<br /> 1,1,1,2-Tetrachloroethane ND 1 0 0 5 1,1,2,2-Tetrachloroethane ND 1 0 0 5
<br /> Tetrachloroethene 1 7 10 0 5 Toluene ND 1 0 0 5
<br /> 1,2,3-Trichlorobenzene ND 10 0 5 1,2,4-Trichlorobenzene ND 1 0 0 5
<br /> 1,1,1-Trichloroethane ND I 10 0 5 1,1,2-Tnehloroethane ND 1 0 0 5
<br /> Trichloroethene ND 10 0 5 Tnehlorofluoromethane ND 1 0 0 5
<br /> 1,2,3-Tnchloro ro ane ND 10 0 5 1,1,2-Tnchloro-1,2,2-tnfluoroethane ND 1 0 10
<br /> 1,2,4-Tnmeth lbenzene ND l 0 0 5 1,3,5-Tnmeth lbenzene ND 1 0 0 5
<br /> Vm 1 Chloride t ND 1 0 0 5 Xylenes ND 1 0 0 5
<br /> Surrogate Recoveries(%)
<br /> %SSI 102 %SS2 97 5
<br /> %SS3 101
<br /> Comments
<br /> *water and vapor samples and all TCLP&SPLP extracts are reported in lig/L,sotUsludge/sohd samples inµg/kg, wipe samples inµg/wipe,
<br /> production/non-aqueous liquid samples in mg/L..
<br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis
<br /> #surrogate diluted out of range or surrogate coelutes with another peak
<br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than--2 vol %sediment,i)sample diluted due to high
<br /> organic content
<br /> DHS Certification No 1644 Rydehus,Lab Manager
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