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116 2nd Avenue South !€D7 Pacheco CA 94553-5560 <br /> E4 McCampbell Analytical Inc Telephone 925-798-1620 Fax 925 798-1622 <br /> httpJ/www m.'c bell com E mail mam mccatnpbell corn <br /> Advanced GeoEnvtrontnental, Inc Client Project ID Cherokee Truck Stop Date Sampled 09/25/03 <br /> 837 Shaw Road Date Received 09/26/03 <br /> Client Contact Paul Dotson Date Extracted 09/30/03-10/01/03 <br /> Stockton,CA 95215 <br /> Client P O Date Analyzed 09/30/03-10/01/03 <br /> Volatiles Organics+Oxygenates by P&T and GC/MS(Basic Target List)* <br /> Extraction Method SW5030B Analytical Method SW826013 Work Order 0309482 <br /> Lab ID 0309482-004C <br /> Client ID UST5 <br /> Matrix Water <br /> 7R Ttgl <br /> Compound Concentration* DF Rep. Compound Concentration * DF .' <br /> Acetone ND<100 20 50 tert-Am l methyl ether KTAME) ND<10 20 05 <br /> Benzene ND<10 20 0 5 Bromobenzene ND<10 20 0 5 <br /> Bromochloromethane ND<10 20 0 5 Bromodichloromethane I ND<10 20 0 5 <br /> Bromoform ND<10 20 0 5 I Bromomethane ND<10 20 0 5 <br /> I 2-Butanone MEK ND<20 20 1 0 j t-Butyl alcohol BA ND<100 20 5 0 <br /> n-But t benzene ND<10 20 0 5 sec-Bu!yl benzene ND<10 20 0 5 <br /> tert-Butyl benzene ND<10 20 0 5 Carbon Disulfide N0<10 20 1 0 5 <br /> Carbon Tetrachloride ND<10 20 0 5 Cblorobenzene ND<10 20 0 5 <br /> I Chloroethane ND<10 20 0 5 2-Chlorueth I Vinyl Ether ND<10 20 0 5 <br /> Chloroform ND<10 20 05 1 Chloromethane ND<10 20 0 5 <br /> 2-Chlorotoluene ND<10 20 0 5 4-Chlorotoluene ND<10 20 05 <br /> Dibromochloromethane ND<10 20 05 1,2-1)lbromo-3-chlororo ane ND<10 20 0 5 <br /> 1,2 Dibromoethane(EDB) ND<10 20 05 Dibromomethane ND<10 20 0 5 <br /> 1,2-Dichlorobenzene ND<10 20 0 5 1,3-Dichlorobenzene ND<10 20 05 <br /> 1,4-Dichlorobenzcne ND<10 20 05 Dichlorodifluoromethane ND<10 20 05 <br /> 1,1-Dichloroethane ND<10 20 05 1,2-Dichloroethane(1,2-DCA)... 510 20 0 5 <br /> 1,1-Dichloroethene ND<l0 20 0 5 cis-1,2-Dichluroethene ND<10 20 05 <br /> trans-l,2-Dichloroethene ND<10 20 0 5 1,2-Dichloro ro ane ND<10 20 05 <br /> 1,3-Dichlororo ane ND<10 20 05 2,2-Dichloropro ane I ND<10 20 1 0 5 <br /> I 1,1-Dichloro ropenc ND<10 20 0 5 cis-1,3-Dichloro ro ene ND<10 i 20 0 5 <br /> trans-l,3-Dichloro ra ene ND<10 20 05 Dusopropyl ether(DIPE) ND<10 I 20 0 5 <br /> Eth�]benzene ND<10 20 05 Ethyl tert-butyl ether(ETBE) ND<10 20 0 5 <br /> HLxachlorobutadiene ND<10 20 10 5 2-Hexanone ND<10 20 0 5 <br /> Iodomethane Methyl iodide) I ND<100 20 I 5 0 Isopropylbcnzene ND<l0 20 0 5 <br /> 4-isopropyl toluene I ND<10 20 10 5 Meth I-t-but t Lther(MTBE) ND<10 20 0 5 <br /> i <br /> Meth leve chloride I ND<10 1 20 0 5 4-Meth I-2- entanone(MIBK NI3<10 20 0 5 <br /> Naphthalene ND<10 20 0 5 I n-Pro yl benzene ND<10 20 0 5 <br />' <br /> Styrene ND<10 20 05 1 l 1,2-Tetrachloroethane ND<10 20 05 <br /> 1 1,2,2-Tetrachloroethane ND<10 20 05 Tetrachloroethenc ND<10 20 05 <br /> Toluene ND<10 20 05 1,2,3-Tnchlnrobenzenc I ND<10 20 05 <br /> 1,2,4-Tnchlorobenzene ND<10 20 05 1,1 1-Trichloroethane NL)<10 20 05 <br /> l 1 2-Trichloroethane ND<10 20 05 Trichloroethene ND<10 20 E 05 <br /> Tnchlorofluoromethane ND<10 20 05 1,2,3-Tnchloro ro ane ND<]0 20 05 <br /> 1,2,4-Tnmethylbenzene NI3<10 20 05 1,3,5-Trimeth ]benzene L ND<10 20 05 <br /> Vinyl Acetate ND<100 20 50 Vinyl Chloride ND<10 20 0 5 <br /> X lenes ND<10 20 I 05 <br /> Surrogate Recoveries(%) <br /> %SS 1 109 %SS2 103 <br />' %SS3 I 923 <br /> Comments <br /> *water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludge/solid samples in pg/kg, wipe samples inµg/wipe, <br /> production/non-aqueous liquid samples in mg/L. <br /> IND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> .#surrogate diluted out of range or surrogate coelutes with another peak <br /> I h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,3)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydelius, Lab Manager <br />