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McCarnpbell Analytical 7ne 110 e epho nue South 16 Pacheco CA 98-16 5560 , <br /> Tele hone 925-798-1620 Fax 925-798-1622 <br /> ht //www nice bell cam E-mail team mcca bell com <br /> FAdvancedGeoEnwrornumental, Inc Client Project ID Cherokee Truck Stop Date Sampled 09/25/03 <br /> 837 Shaw Road Date Received 09/26/03 <br /> Client Contact Paul Dotson Date Extracted 09/30/03-10/01/03 <br /> Stockton,CA 95215 <br /> Client P ODate Analyzed 09/30/03-10101103 <br /> I Volatiles Organics+Oxygenates by P&T and GC/MS(Basic Target List)* <br /> Extraction Method SW5030B Analytical Method SW8260B Work Order 0309482 <br /> Lab ID 0309482-005C <br /> Client ID UST6 <br /> Matrix Water <br /> Compound Concentration * DF °y° s Compound Concentration* DF R`�,m,�g <br /> Acetone ND 1 0 1 50 tert-Am 1 methyl ether(TAME) ND 10 05 <br /> Benzene ND 1 0 0 5 Bromobenzene ND 1 0 0 5 <br /> Bromochloromethane ND 1 0 0 5 Broinodichloromethane ND 10 0 5 <br /> Bromoform ND 1 0 0 5 Bromomethane ND 10 0 5 <br /> 2-Butanone(MEK) ND 1 0 1 0 t-Butyl alcohol(TBA) ND 10 50 <br /> n-Butyl benzene ND 1 0 0 5 ser-Butyl benzene ND 1 0 0 5 <br /> tert-But l benzene ND 1 0 0 5 Carbon Disulfide ND 1 0 0 5 <br /> Carbon Tetrachloride ND 10 05 Chlorobenzene ND 1 0 0 5 <br /> Chloroethane ND 1 0 0 5 2-Chloroethyl Vinyl Ether ND 1 0 0 5 <br /> Chloroform ND 1 0 0 5 Chloromethane ND 10 0 5 <br /> 2-Chlorotoluene ND 10 0 5 4-Chlorotoluene ND 1 0 0 5 <br /> Dibromochloromethane ND 1 0 05 1,2-Dibromo-3�hloro roane ND 1 0 0 5 <br /> 1,2-Dibromoethane EDA ND 1 0 05 Dibromomethane ND 1 0 0 5 <br /> 1 2-Dichlorobenzene ND 1 0 0 5 1,3-Dichlorobenzene ND 1 0 05 <br /> 1,4-Dichlorobenzene ND l 0 0 5 Dichlorodifluoromethane ND 1 0 0 5 <br /> 1,1-Dichloroethane ND 1 0 05 1 2-Dichloroethane 1 2-DCA) 4 4 1 0 05 <br /> 1,1-Dichloroethene ND l0 05 cis-1,2-Dichloroethcnc ND 10 05 <br /> trans-l,2-Dichloroethene ND 1 0 0 5 1,2-Dichlororo ane ND 1 0 0 5 <br /> 1,3-Dichlororo ane ND 1 0 0 5 2,2-Dichloro roane ND 1 0 0 5 <br />' 1 1-Dichloro ro ene ND 1 0 0 5 1 cis-i,3-Dichloro ro ene ND 1 0 0 5 <br /> trans-1 3-Dichloro ro ene ND 1 0 0 5 Dusa ra 1 ether(DIPS) ND ) o 05 <br /> Ethylbenzene ND 1 0 05 Ethyl tert-butyl ether(FTBE) ND 10 0 5 <br /> Hexachlorobutadienc ND 1 0 0 5 2-Hexanone ND i 0 1 05 <br />' lodomethane(Methyl iodide ND 1 0 50 1so ro ylbenzene ND to o5 <br /> 4-1so roT <br /> t toluene ND 1 0 0 5 Meth i-t-but l ether MBE 072 10 05 <br /> Methylene chloride ND 1 0 0 5 4-Meth 1-2- entanone MIBK ND 1 0 0.� <br /> Naphthalene ND 1 0 0 5 n-Propyl benzene ND l 0 0 5 <br />' <br /> Styrene ND 1 0 0 5 1 11,2-Tetrachloroethane ND 1 0 0 5 <br /> 1,1,2,2-Tetrachloroethane ND 1 0 05 Tetrachioroethene ND to 05 <br /> Toluene ND T-10 05 1,2,3-Tnehlorobenzene ND l 0 05 <br /> 1,2,4-Trichlorobenzene_ ND 1 0 05 1 1,1-Trichloroethane ND to 0 5 <br />' l,1 2-Trichloroethane ND 10 05 Trichloroethene ND l 0 0 5 <br /> Trichlorofluoromethane ND 1 0 _05 1,2 3-Tnchloro ro ane ND 10 05 <br /> 1,2,4-Tnmeth lbenzene ND 1 0 05 1,3,5-Tnmeth lbenzene ND 1 0 0 5 <br /> Vinyl Acetate ND l 0 50 Vm 1 Chloride ND I 10 05 <br />' <br /> Xylenes I ND I I O 05 <br /> Surrogate Recoveries(%) <br /> %S S 1 109 %552 100 <br /> %SS3 907 <br />' Comments <br /> water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludge/solid samples in Itg/kg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> 0 #surrogate diluted out of range or surrogate coelutes with another peak <br />' h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,,])sample diluted due to high <br /> organic content <br />' DHS Certification No 1644 Angela Rydellus, Lab Manager <br />