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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hJW//wri)y mccarn eil com E-mail main@mccampbell com <br /> • <br />' Advanced GeoEnvironrnental Client Project ID West Clay Date Sarnpled 03/13/01 <br /> 837 Shaw Road Date Received 03/15/01 <br /> Stockton, CA 95215 Client Contact Paul Dotson Date Extracted 03/16-03/21/01 <br /> Client P O LDateAnalyzed 03/16-03/21/01 <br /> 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> I Lab ID 62696 62697 62698 62699 <br /> MWSB/ MW9/ MWIO/ MW11A/ Reporting Limit <br /> Client ID 031301 03130I 031301 031301 <br />' Matrix W W W W S w <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(D1PE) ND ND<2 5 ND ND 50 10 <br />' Ethyl tert-Butyl Ether(ETBE) ND ND<2 5 ND ND 50 10 <br />' Methyl-tert Butyl Ether(MTBE) ND 140 26 ND 50 10 <br /> tert-Amyl Methyl Ether(TAME) ND ND<2 5 ND ND 50 1 0 <br />' tert-Butanol ND ND<12 5 ND ND 25 50 <br />' Methanol ND ND<500 ND ND 1000 200 <br /> Ethanol ND ND<125 ND ND 250 50 <br /> Surrogate Recoveries(%) <br />' Dlbromofluoromethane 105 107 107 105 <br />' Comments h <br /> " water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP!STLC/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present,(i)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br />' high organic content <br />' DHS Certification No 1644 Edward Hatnilton,Lab Director <br />