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' 110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAA4PBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br />' h //www mccam ll c m E-mail main@mccampbell cam <br /> if <br />' Advanced GeoEnvironmental Client Project ID West Clay Date Sampled 03/13/01 <br /> 837 Shaw Road Date Received 03/15/01 <br />' Stockton, CA 95215 Client Contact Paul Dotson Date Extracted 03/16-03/21/01 <br /> Client P O Date Analyzed 03/16-03121/01 <br />' 7 Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br />' Lab ID 62700 62701 62702 62703 <br /> MWIIB/ MW12A/ MW12B/ MW13A/ Reporting Limit <br /> Client ID 031301 031301 031301 031301 <br />' Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Dt-isopropyl Ether(DIPS) ND ND ND ND 50 10 <br /> Ethyl tent-Butyl Ether(ETRE) ND ND ND ND 50 1 0 <br /> Methyl-tert Butyl Ether(MTBE) 31 ND 93 50 50 10 <br /> lie <br /> tert-Amyl Methyl Ether(TAME) ND ND ND ND 5 0 1 0 <br />' tert-Butanol 12 ND ND ND 25 50 <br />' Methanol ND ND ND ND 1000 200 <br /> Ethanol ND ND ND ND 250 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 107 115 106 116 <br /> Comments <br /> *water samples are reported in ug/L,sod and sludge samples 1n ug/kg,wipes in ug/wipe and all TCLP 1 STLC/SPLP extracts in ug/L <br />' NIS means not detected above the reporting limit N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present (1)liquid sample that contains greater than—5 vol %sediment,0)sample diluted due to <br />' high organic content <br />' DHS Certification No 1644 �Edward Hamilton,Lab Director <br />