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t110 2nd Avenue South #D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 425-798-1622 <br /> http.//wwwr=campbcJIcorn Email niam@mccbcficom <br /> Advanced GeoEnvironmental, Inc Client Project ID West Clay Date Sampled 12/26/02 <br /> 837 Shaw Road Date Received 12/27/02 <br />' Stockton,CA 95215 Client Contact Paul Dotson Date Extracted 12/27/02 <br />' <br /> relle-nip O Date Analyzed 12/27/02-12/30/02 <br /> Oxygenates and BTEX by GC/MS* <br /> Eadracnon Method SW5030B Analytical Mctho&SW8260B Work Order 0212433 <br />' Lab ID 0212433-009B 0212433-010B 10212433-OIIB 0212433-012B <br /> Client ID MW-8A MW-8B MW-9W-10 Reporting Limit for <br /> DF=1 <br /> Matrix W W I W iW <br /> - — - <br /> DE 1 1 i 10 2 S W <br /> Compound Concentration ug(Kg llg/L <br />' tert-Amyl methyl ether(TAME) ND ND NIKS 0 ND<l NA 05 <br /> Benzene ND ND ND<5 0 12 NA 0 5 <br />' t-Butyl alcohol(TBA) ND ND ND<50 ND<10 NA 5 0 <br /> 1,2-Dibromoethane(EDB) ND ND ND<5 0 ND<1 NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) 0 54 ND ND<5 0 ND<l NA 0 5 <br />' Dusopropyl ether(DIPE) ND ND ND<5 0 ND<l NA 0 5 <br /> Ethanol ND ND ND<500 ND<100 NA 50 <br /> Ethylbenzene ND ND ND<5 0 68 NA 05 <br />'. Ethyl tert-butyl ether(ETBE) ND ND ND<5 0 ND<1 NA 0 5 <br /> Methanol ND ND ND<5000 ND<1000 NA 500 <br /> Methyl-t-butyl ether(MTBE) ND ND 130 34 NA 0 5 <br />' Toluene ND ND ND<5 0 ND<l NA 05 <br /> Xylenes ND ND ND<5 0 7 2 NA 05 <br /> Surrogate Recoveries(%) <br /> I %SS 998 99 3 108 108 <br /> Comments �p <br /> "water and vapor samples and all TCLP&SPLP extracts are reported in pg/L,soil/sludge/solid samples inµg/kg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br />' h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than—2 vol %sediment,J)sample diluted due to high <br /> o anic content <br /> I <br /> I <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />