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' 110 2nd Avenue South,##D7 Pacheco CA 94553-5560 <br /> McCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> h J/www mcc bell cam E-mail bell corn <br /> Advanced GeoEnvironmental,Inc Client Project ID West Clay Date Sampled 12/26/02 <br />' 837 Shaw Road Date Received 12/27/02 <br /> Stockton, CA 95215 Client Contact Paul Dotson Date Extracted 12/27/02 <br />' <br /> rChent P O Date Analyzed 12/27/02-12/30/02 <br /> Oxygenates and BTEX by GC/MS* <br /> Extraction Method SW5030B Analytical Method SW9260B Work Order 0212433 <br />' Lab ID 0212433-013B 0212433-014B 0212433-015B 0212433-016B <br /> CIient ID MW-IIA MW-118 MW-12A MW-12B Reporting Limit for <br /> ----- ------- -- -— -- DF=i <br /> Matrix W W W W <br />' DF 1 - 2 - - 1— 1 S W <br /> Compound Concentration Rg/Kg µgR- <br />' Cert-Amyl methyl ether(TAME) ND ND<I ND ND NA 05 <br /> Benzene ND ND<l ND ND NA 0 5 <br />' t-Butyl alcohol(TBA) ND ND<10 ND ND NA 50 <br /> 1 2-Dibromoethane(EDB) ND ND<i ND ND NA 05 <br /> 1,2-Dichloroethane(1,2-DCA) ND 14 ND 15 NA 0 5 <br /> Ditsopropyl ether(DIPS) ND ND<I ND ND NA 05 <br /> Ethanol ND ND<100 ND ND NA 50 <br /> Ethylbenzene ND ND<I ND ND NA 05 <br /> Ethyl tent-butyl ether(ETBE) ND ND<1 ND ND NA 010 5 <br /> Methanol ND ND<1000 ND ND NA 500 <br /> Methyl-t-butyl ether(MTBE) ND 34 ND 47 NA 0 5 <br />' Toluene ND ND<l 0 ND ND NA 0 5 <br /> Xylenes ND ND<1 ND ND NA 0 5 <br /> Surrogate Recoveries(%) <br />' %SS 979 108 989 95 7 <br /> Comments <br />' •water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,soil/sludge/solid samples inµg/kg, wipe samples inµg/wipe, <br /> product/oil/non-aqueous liquid samples in mg/L <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> h)lighter than water immiscible sheen/product is present,i)liquid sample that contains greater than-2 vol %sediment,J)sample diluted due to high <br /> organic content <br /> I <br /> DHS Certification No 1644 Edward Harmlton,Lab Director <br /> I <br />