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Alpha Analytical, Inc. <br /> 255 Glendale Ave.• Suite 21 • Sparks, Nevada 89431-5778 <br /> 1 (775)355-1044•(775)355-0406 FAX• 1-800-283-1183 <br /> —Afk <br /> D81e: OC Summary Report Work Order: <br /> I7-Jun-08 08060609 <br /> ethed Blank Type MBLK Test Code: EPA Method SW8260B <br /> ile ID:08061107.D Batch ID:MSISS0053A Analysis Date: 081111200811:08 <br /> Sample ID: MBLK MS1550053A Units: pg/Kg Run ID:MSD_15_080611A Prep Dale: 06/11/2008 <br /> analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> enzene NO 5 <br /> Toluene NO 5 <br /> 1thylbenzene NO 5 <br /> p-Xvlene ND 5 <br /> -Xylene ND 5 <br /> Surr: 1,2-Dichloroethane-d4 190 200 95 69 126 <br /> Surf:Toluene-d8 206 200 103 80 120 <br /> purr:4-Bromofluorobenzene 189 200 95 80 120 <br /> IllLaboratory Control Spike Type LCS Test Code: EPA Method SW8260B <br /> File ID:08061104.D Batch ID:MS15SO053A Analysis Date: 0611112008 10:02 <br /> ample ID: LCS MS15SO053A Units: pg/Kg Run ID:MSD_15_080611A Prep Date: 06/1112008 <br /> nalyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> Benzene 406 10 400 102 70 140 <br /> oluene 392 10 400 98 70 130 <br /> thylben <br /> zene 419 10 400 105 70 1300 <br /> ,p-Xylene 433 10 400 108 70 133 <br /> o-Xylene 440 10 400 110 70 135 <br /> Sum: 1,2-Dichloroethane-d4 355 400 89 69 126 <br /> urr:Toluene-d8 405 400 101 80 120 <br /> urr:4-BromoOuorobenzene 385 400 96 80 120 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW8260B <br /> OHe ID:08061115.D Balch ID:MS15SO053A Analysis Date: 061111200814:09 <br /> ample ID: 08053058-16AMS Units: pg/Kg Run ID:MSD_15_080611A Prep Date: 06/11/2008 <br /> nalyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> Benzene 340 10 400 0 85 57 140 <br /> ohlbe <br /> luene 329 10 400 0 82 60 130 <br /> tyn <br /> zene 364 10 400 0 91 63 1344 <br /> .P-Xylene 365 10 400 0 91 64 136 <br /> o-Xylene 366 10 400 0 92 62 138 <br /> Eurr: 1,2-Dichloroethane-d4 352 400 88 69 126 <br /> urr:Toluene-d8 403 400 101 80 120 <br /> un:4-Bromofluorobenzene 390 400 98 80 120 <br /> Sample Matrix Spike Duplicate Type MSD Test Code:EPA Method SW82608 <br /> He ID:08061116.D Batch ID:MS15S0053A Analysis Date: 06/11/200814:32 <br /> ample ID: 08053058-16AMSD Units:pg/Kg Run ID:11508061 IIA Prep Date: 0611112008 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> enzene 393 10 400 0 98 57 140 340.5 14.3(20) <br /> oluene 378 10 400 0 95 60 130 329.5 13.8(20) <br /> thylbenzene 409 10 400 0 102 63 134 364.4 11.5(20) <br /> m,p-Xylene 410 10 400 0 103 64 136 364.6 11.8(20) <br /> Xylene 415 10 400 0 104 62 138 366.4 12.4(20) <br /> urr: 1,2-Dichloroethane-d4 349 400 87 69 126 <br /> urr:Toluene-d8 402 400 101 80 120 <br /> Surr:4-Bromofluorobenzene 394 400 99 80 120 <br /> 'ornments: <br /> 'alculations are based o0-of raw(non-rounded)dam. However,for reporting purposes.all QC data is rounded to three significant figures.Therefore,hand calculated <br /> values may differ slightly. <br /> I <br /> 1 <br /> 1 <br />