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' A Alpha Analytical, Inc. <br /> 255 Glendale Ave. •Suite 21 •Sparks, Nevada 89431-5778 <br /> (775)355-1044 •(775)355-0406 FAX• 1-800-283-1183 <br /> ' <br /> 08 Date: OC Summary Report Work Order: <br /> 13-Jun- 08060609 <br /> Iethod Blank Type MBLK Test Code: EPA Method SW6020/SW6020A <br /> le ID: 060908.Bk005SMPL.Dt Batch ID: 20051 Analysis Dale: 06110/2008 11:50 <br /> Sample ID: MB-20051 Units : mg/Kg Run ID:ICPIMS_080609C Prep Date: 0610912008 <br /> alyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> ryllium (Be) ND 1 <br /> nadium(V) ND 1 <br /> Chromium(Cr) ND 1 <br /> balt(Co) ND 1 <br /> CClow(Ni) ND 2 <br /> low(Cu) ND 2 <br /> Zinc(Zn) ND 20 <br /> Arsenic(As) ND 1 <br /> lenium(Se) ND 1 <br /> olybdenum(Mo) ND 1 <br /> Silver(Ag) ND 1 <br /> Cadmium(Cd) ND 1 <br /> imony(Sb) ND 1 <br /> erium (Ba) ND 11 <br /> rcury(Hg) ND 0.2 <br /> Thallium(TI) ND 1 <br /> It ad (Pb) ND 1 <br /> laboratory Control Spike Type LCS Test Code: EPA Method SW6020/SW6020A <br /> File ID:060908.B%A092_LCS.D Batch ID:20051 Analysis Date: 0610912008 23:20 <br /> mple ID: LCS-20051 Units: mg/Kg Run ID:ICP/MS 080609C Prep Date: 0610912008 <br /> ialyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> eryllium(Be) 25 1 25 100 77 124 <br /> Vanadium(V) 25 1 25 99.9 72 120 <br /> thromium(Cr) 24.8 1 25 99 75 120 <br /> bait(Co) 24.3 1 25 97 74 120 <br /> ickel(Ni) 25.7 2 25 103 80 124 <br /> Copper(Cu) 25.3 2 25 101 80 125 <br /> nc(Zn) 25.6 20 25 102 73 135 <br /> senic(As) 25.2 1 25 101 80 120 <br /> lenium (Sal 25.3 1 25 101 80 120 <br /> Molybdenum(Mo) 24.5 1 25 98 77 120 <br /> Silver(Aq) 23.4 1 25 94 62 132 <br /> dmium(Cd) 25 1 25 100 80 120 <br /> timony(Sb) 20.4 1 25 82 53 124 <br /> arium(Ba) 265 1 250 106 78 123 <br /> Mercury(Hq) 0.464 0.2 0.5 93 68 140 <br /> [allium ITI) 24.5 1 25 98 73 120 <br /> ad(Pb) 25.4 1 25 101 80 122(Pb) 25.4 1 25 101 80 122 <br /> Sample Matrix Spike Type MS Test Code: EPA Method SW6020/SW6020A <br /> ile ID:060908.B1A095SMPL.D Batch ID:20051 Analysis Date: 06/0912008 23:36 <br /> mple ID: 08060609-01AMS Units : mg/Kg Run ID:ICP/MS-080609C Prep Date: 06/0912008 <br /> nalyle Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> Beryllium (Be) 24.6 1 25 0 98 75 132 <br /> anadium(V) 39.2 1 25 13.01 105 50 150 <br /> 11hromium(Cr) 33.7 1 25 9.301 98 50 150 <br /> obalt(Co) 26.2 1 25 3.168 92 62 130 <br /> Nickel(Ni) 33.8 2 25 11.79 88 50 149 <br /> opper(Cu) 33.3 2 25 3.554 119 54 143 <br /> nc(Zn) 37.9 20 25 0 152 50 147 Mi <br /> rsenic(As) 25.8 1 25 1.9 96 60 130 <br /> Selenium (Se) 24.2 1 25 0 97 69 130 <br /> olybdenum (Mo) 25.1 1 25 0 100 70 130 <br /> ilver(Aq) 23.3 1 25 0 93 62 132 <br /> admium (Cd) 25 1 25 0 100 70 130 <br /> Antimony(Sb) 20.8 1 25 0 83 50 130 <br /> Barium(Ba) 296 1 250 30.87 106 58 150 <br /> ercury(Hq) 0.455 0.2 0.5 0 91 65 150 <br /> hallium(TI) 24.1 1 25 0 96 70 130 <br /> ead(Pb) 28.5 1 25 2.203 105 68 141 <br />