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1 4& Alpha Analytical, Inc. <br /> 255 Glendale Ave. •Suite 21 •Sparks, Nevada 89431-5778 <br /> (775)355-1044 •(775)355-0406 FAX • 1-800-283-1183 <br /> ! Date:- OC Summary Report 08060609 <br /> ork Order: <br /> l?-Jun-08 03060609 <br /> tmple Matrix Spike Duplicate Type MSD Test Code: EPA Method SW60201 SW6020A <br /> le ID:060908.BV1096SMPL.D Batch ID:20051 Analysis Date: 06/09/2008 23:42 <br /> Sample ID: 08060609-01AMSD Units: mg/Kg Run ID:ICP/MS-080609C Prep Date: 06109/2008 <br /> Wipalyte Result PQL SpkVal SpkRefVal %REC LCL(ME) UCL(ME)RPDRefVal %RPD(Limit) Qual <br /> Raryllium(Be) 25 1 25 0 100 75 132 24.58 1.7(20) <br /> nadium(V) 40.2 1 25 13.01 109 50 150 39.22 2.6(20) <br /> Chromium(Cr) 36.6 1 25 9.301 109 50 150 33.74 8.1(20) <br /> Ipbalt(Co) 26.8 1 25 3.168 95 62 130 26.17 2.4(20) <br /> ckel(Ni) 34.9 2 25 11.79 92 50 149 33.8 3.1(20) <br /> Aper(Cu) 28.5 2 25 3.554 99.9 54 143 33.31 15.4(20) <br /> Zinc(Zn) 37.3 20 25 0 149 50 147 37.92 1.6(20) M1 <br /> enic(As) 26.7 1 25 1.9 99 60 130 25.8 3.4(20) <br /> renium (Se) 25 1 25 0 99.9 69 130 24.24 3.0(20) <br /> l <br /> lybdenum(Me) 25.6 1 25 0 102 70 130 25.11 2.0(20) <br /> Silver(Aq) 23.7 1 25 0 95 62 132 23.34 1.6(20) <br /> miumny (Cd) 25.5 1 25 0 102 70 130 24.99 2.1(20) <br /> timotl (Sb) 21.9 1 25 0 88 50 130 20.81 5.3(20) <br /> rium (Be) 301 1 250 30.87 108 58 150 296.3 1.6(20) <br /> Mercury ft) 0.469 0.2 0.5 0 94 65 150 0.455 3.1(20) <br /> Thallium(TI) 25.3 1 25 0 101 70 130 24.12 4.7(20) <br /> Itad(Pb 28.4 1 25 2.203 105 68 141 28.54 0.5(20) <br /> omments: <br /> Calculations are based off of raw(non-rounded)data.However,for reporting purposes,all QC data is rounded to three significant figures.Therefore.hand calculated <br /> lues may difler slightly. <br /> 1 =Matrix spike recovery was high,the method control sample recovery was acceptable. <br /> ! <br /> ! <br /> 1 <br /> 1 <br /> 1 <br /> 1 <br /> 1 <br /> 1 <br />