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E <br /> On December 19,,1994,a agger excavator performed additional excavation downward <br /> and toward the south, according to the recommendation of Mr. Snavely. This <br /> recommendation was the result of review of the analyses of the samples collected at 11.0 <br /> ft, and the information provided by diesel fuel staining within the excavation. <br /> Sample TK04-829-01-D1U1-SO-17.0 was collected on December 19 and submitted to <br /> CLS for TPH-D and BTXE analyses. The results of analyses showed 2400 mg/kg TPH- <br /> D,and 0.042 mg/kg for xylene of the BTXE analytes. <br /> Noting that the TPH-D concentration for the soil sample collected at a depth of 17.0 feet <br /> was fifty percent greater than the value for the sample collected at depth of 11.0 feet, an <br /> investigation was initiated to learn more about causes for the apparent increase in <br /> concentration with increasing depth. We determined that the analytical laboratory <br /> (CLS) collected a 5.0 gram sample from our sample tube without regard to the fact that <br /> the tube contained a stratified composite sample. The stratified composite consisted of <br /> several strata collected from several locations within the back hoe bucket to represent <br /> both the stained and unstained portions of the soil within the bucket. On December 27, <br /> 1994,CLS was asked to homogenize the remaining sample (all present except for the <br /> five grams used in the initial analysis) and perform a second TPH-D analysis. (A <br /> second BTXE analysis was not requested because of the time elapsed since sample <br /> collection.) The result of the re-analysis of sample TK04-829-01-D1U1-SO-17.0) showed <br /> 990 mg/kg TPH-D. <br /> In order to improve our understanding of the amount of diesel fuel contamination <br /> remaining in the tank removal excavation, additional soil samples were collected from <br /> the bottom of the excavation on December 21, 1994. Sample TK05-829-01-D1U1-SO-17.0 <br /> was analyzed by CLS and showed 58.0 mg/kg TPH-D and ND for BTXE. Sample TK06- <br /> 829-01-D1U1-SO-17.0 was analyzed by GTEL Environmental Laboratories,Inc.,in <br /> Concord,Ca.,and showed 930 mg/kg TPH-D and ND for BTXE. Sample TK07-829-01- <br /> D1U1-SO-17.0 was submitted to CLS and showed 630 mg/kg for TPH-D and 0.033 <br /> mg/kg xylene of the BTXE analyte. The GTEL sample analyses (not a split sample)was <br /> performed to provide an informal check against the CLS analyical results. <br /> Please note the attached table"Summary of 829-DlU1 Tank Closure Soil Sample <br /> Analyses Results". <br /> The at the 829-DlU1 closure site "VicMat below the <br /> surface rsonal communication withrid and Mike Taffet <br /> of the Lawrence Livermore National Laboratory Environmental Protection Department, <br /> Environmental Restoration Division. This information is based on monitoring well <br /> data.) <br />