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Alpha Analytical, Inc. 255 Glendale Ave •Suite 21 • Sparks, Nevada 89431-5778 (775) 355-1044 •(775)355-0406 FAX • 1-800-283-1183 I I ate 08-MuWork Order v 03 QC Summary Report 03050540 ' Sample Matrix Spike Type MS Test Code EPA Method SW82608 File ID C IHPCHEM1MS011DATA1030505103050528 D Batch ID MSIW0505A Analysis Date 05/05/2003 22 19 ' Sample ID 03050228-02AMS Units pg1L Run 1D GCIMSD_1_030505A Prep Date 05/05/2003 Analyte Result PQL SpkVal SpkRefVal %REC LowLimlt HighLimit RPD Ref Val %RPD Quaf 1 1-Dichloroethene 45 7 2 5 50 0 91 80 120 ' Benzene 443 1 3 50 0 89 83 919 Trichloroethene 388 2 5 50 0 78 76 127 Toluene 408 1 3 50 0 82 80 120 Chlorobenzene 416 2 5 50 0 83 76 124 Ethylhenzene 41 13 50 0 82 80 120 m p-Xylene 766 1 3 100 0 77 77 124 o-Xylene 387 1 3 50 0 77 77 125 Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B ' File ID C IHPCHEMIMS011DATA1030505103050529 D Batch ID MSlW0505A Analysis Date 05/05/2003 22 44 Sample ID 03050228-02AMSD Units pg/L Run ID GC/MSD 9 030505A Prep Date 0510512003 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Highl-imit RPD Ref Val %RPD Qua] ' 1 1-Dichloroethene 542 25 50 0 108 80 120 4573 17 Benzene 521 1 3 50 0 104 83 119 443 161 Trichloroethene 503 2 5 50 0 101 76 127 388 257 Toluene 503 1 3 50 0 101 80 120 4077 20 9 Chlorobenzene 504 2 5 50 0 101 76 124 41 58 192 Ethylbenzene 48 2 1 3 50 0 96 80 120 41 04 161 m,p-Xylene 922 1 3 100 0 92 77 124 7661 184 o-Xylene 472 1 3 50 0 94 77 125 3872 197 ments ND-Not Detected at the Reporting Limit D If the spiked value is<25%of the reference value,recovery should not be calculated md S-Spike Recovery outside accepted recovery limas M-Spike Recovery outside accepted recovery limits due to matrix B-Analyte detected in the associated Method Blank i 1 1 1 I 1 I I