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Alpha Analytical, Inc. 255 Glendale Ave •Suite 21 •Sparks,Nevada 89431-5778 z (775)355-1044 •(775)355-0406 FAX - 1-800-283-1183 ate ' 08-Mav-03 QC Summary Report Work Order 03050540 Method Blank Type MBLK Test Code EPA Method SW8015 File 0 C IHPCHEMkMSO1kDATAkO30505103050507 D Batch ID MSIW0505B Analysis Date 05105/2003 13 16 ' Sample ID MBLK MSlWO505A Units mg1L Run ID GC/MSD_I-030505A Prep Date 05/05/2003 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual TPH Purgeable NO 005 Laboratory Control Spike Type LCS Test Code EPA Method SW8015 File ID C IHPCHEMIMS01kDATA1O3O505kO3050505 D Batch ID MS1W0505B Analysis Date 05/0512003 12 25 Sample ID GLCSWMS1W0505B Units mg1L Run ID GC/MSD_i_030505A Prep Date 05/05/2003 Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Highl-imit RPD Ref Val %RPD Qual TPH Purgeable i g 0 461 005 04 115 58 136 Sample Matrix Spike Type MS Test Code EPA Method SW8015 ' File ID C IHPCHEMIMS01kDATA1030505k03050530 D Batch ID MSIW0505B Analysis Date 05/05/2003 23 10 Sample ID 03050228-02AGS Units mglL Run ID GCIMSD_I-030505A Prep Date 05/05/2003 Analyte Result PQL SpkVal SpkRefVal %REC Lowt-imd Hight-imit RPD Ref Val %RPD Qual ' TAH Purqeable 217 025 2 0 109 58 136 Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8015 He ID C kHPCHEMIMS01kDATAkO30505kO305O531 D Batch ID MSIW0505B Analysis Date 05/05/2003 23 36 ' Sample ID 03050228-02AGSD Units mg1L Run ID GCIMSD_1_030505A Prep Date 05/05/2003 Ana?yte Result PQL SpkVal SpkRefVal %REC Lowl-imit Hight-imit RPD Ref Val %RPD Qua] TPH Purgeable 235 025 2 0 118 58 136 217 802 wments ND-Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matrix B Analyte detected in the associated Method Blank 1 1 1