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Alpha Analytical, Inc. 255 Glendale Ave •Suite 21 •Sparks,Nevada 89431-5778 (775)355-1044 •(775) 355-0406 FAX • 1-800-283-1183 ate Work Order 14-Apr 03 QC Summary Report W03040601 Method Blank Type MBLK Test Code EPA Method SW6020 File ID 040703 B1054_ICB D1 Batch 10 7673 Analysis Date 04107/2003 15 18 ' Sample ID MB-7673 Units mg1L Run ID tCPIMS_030407B Prep Date 04/07/2003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Hight-emit RPD Ref Val %RPD Qual Lead NO 0 005 I ' Laboratory Control Spike Type LCS Test Code EPA Method SW6020 File ID 040703 81055_LCS D4 Batch ID 7673 Analysis Date 04/07/2003 15 22 Sample ID LCS-7673 Units mglL Run ID ICP/MS 030407E Prep Date 04/03/2003 ' Analyte Result PQL SpkVal SpkRefVal %REC Lowbmit HighLimit RPD Ref Val %RPD Qual Lead 0 243 0 005 025 97 85 115 Sample Matrix Spike Type MS Test Code EPA Method SW6020 File ID 040703 B1058SMPL DI Batch ID 7673 Analysis Date 04/07/2003 15 35 Sample ID 03032644-01AMS Units mglL Run ID WP1M5_030407B Prep Date 04/03/2003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual ' Lead 023 0 005 025 0 92 70 130 Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW6020 File 10 040703 B1001SMPL DI Batch ID 7673 Analysis Date 0410712003 16 10 ' Sample ID 03032644-01AM5D Units mg/L Run ID ICPIMS_030407B Prep Date 04/0312003 Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual Lead 0 226 0 005 025 0 90 70 130 02299 162 moments NO-Not Detected at the Reporting Limit D-if the spiked value is<25%of the reference value,recovery should not be calculated S-Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matnx B-Analyte detected in the associated Method Blank I I i I 1