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1 Alpha Analytical, Inc. <br /> 255 Glendale Ave •Suite 21 •Sparks, Nevada 89431-5778 <br /> (775)355-1044 •(775)355-0406 FAX - 1-800-283-1183 <br /> PDate 'Work Order <br /> t14-Apr 03 QC Summary Report 03040601 <br /> Method Blank Type MBLK Test Code EPA Method SW8015 <br /> File 10 D kHPCHEM1MS09kDATAk03O4O7kO3O4O7O8 D Batch ID MS9SO407B Analysis Date 04/0712003 11 37 <br /> Sample ID MBLK MS9SO407A Units mglKg Run ID GC/MSD-9-030407A Prep Date 04/07/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowt-emit HighUrnit RPD Ref Val %RPD Qual <br /> TPH Purgeable ND t <br /> ' Laboratory Control Spike Type LCS Test Code EPA Method SW8015 <br /> File ID D 1HPCHEM1MS091DATA1030407103040712 D Batch ID MS9SO407B Analysis Date 04107/2003 13 11 <br /> Sample ID GLCS MS9SO407B Units mg/Kg Run 10 GCIMSD_9_030407A Prep Date 04107/2003 <br /> ' Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br /> TPH Purgeable 826 1 8 103 61 144 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8015 <br /> ' File ID D 1HPCHEM%MS091DATA1030407103040715 D Batch ID MS9SO407B Analysis Date 04/07/2003 14 21 <br /> Sample ID 03040601-OSAGS Units mglKg Run ID GCIMSD_9_030407A Prep Date 04/0712003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> ' TPH Purqeable 661 1 8 0 83 61 144 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8015 <br /> File ID D IHPCHEM1MS091DATA1030407103040716 D Batch ID MS9SO407B Analysts Date 04/0712003 14 45 <br /> ' Sample ID 03040601-OSAGSO Units mg/Kg Run ID GC/MSO-9-030407A Prep Date 04/07/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual <br /> TPH Purgeable 751 1 8 0 94 61 144 6 605 129 <br /> �mments ND-Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated - <br /> S Spike Recovery outside accepted recovery limits M-Spike Recovery outside accepted recovery limits due to matnx <br /> H-Analyte detected in the associated Method Blank <br /> t <br /> 1 _ <br /> 1 <br /> 1 <br /> 1 I <br />