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OULAB CORE LABORATORIES S u R R 0 G A T E R F C 0 V E R I E S R E P O R T Job Number 990931 Report Date 05/31/1999 CUSTOMER IT Group PROJECT- Southland - Martinez ATTN Bob Butler Method Volatile Organics -Aromatics Batch 6447 Method Code 80208X Analyst evd Surrogate Units 4-Bromofluorobenzene ug/L Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time MB 1 44 95 50 0000 89 9 64-147 05/26/1999 1000 LCS 1 47 86 50 0000 95 7 64-147 05/26/1999 1329 LCD 1 49 89 50 0000 99 8 64-147 05/26/1999 1354 990931-2 Liquids 1 46 67 50 0000 93 3 64-147 05/26/1999 1512 1990931-3 Liquids 1 45 34 50 0000 90 7 64-147 05/26/1999 1539 990931-4 Liquids 1 49 16 50 0000 98 3 64-147 05/26/1999 1605 19911932-1 Liquids 1 53 47 50 0000 106 9 64-147 05/26/1999 1631 990932-2 Liquids 1 45 37 50 0000 90 7 64-147 05/26/1999 1657 990932-3 Liquids 1 50 88 50 0000 101 8 64-147 05/26/1999 1723 990933-8 Liquids 1 43 45 50 0000 86 9 64-147 05/26/1999 2326 10933-9 Liquids 1 42 73 50 0000 85 5 64-147 05/26/1999 2352 08-4 Solid 5 43 37 50 0000 86 7 64-147 05/27/1999 0018 31-2 Liquids MS 1 47 84 50 0000 95 7 64 147 05/27/1999 0136 31-2 Liquids MSD 1 47 61 50 0000 95 2 64 147 05/27/1999 0202 990877-16 5 45 14 50 0000 90 3 64-147 05/27/1999 0411 Method Volatile Organics -Aromatics Batch 6461 Method Code 8020BX Analyst evd Surrogate Units 4-Bromofluorobenzene ug/L Lab IU Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time 990931-2 Solid MS 1 47 842 50 0000 95 7 64-147 05/26/1999 0136 90931-2 Solid MSB 1 47 612 50 0000 95 2 64-147 05/26/1999 0202 90931-2 Solid 1 46 672 50 0000 93 3 64-147 05/26/1999 1512 9 2 MB 1 42 56 50 0000 85 1 64-147 05/27/1999 1149 LCS 1 46 66 50 0000 93 3 64-147 05/27/1999 1307 LCD 1 45 62 50 0000 91 2 64-147 05/27/1999 1333 0990931-1 Liquids 5 43 05 50 0000 86 1 64-147 05/27/1999 1519 90932-3 Liquids 5 44 62 50 0000 89 2 64-147 05/27/1999 1545 990932-5 Liquids 25 47 39 50 0000 94 8 64-147 05/27/1999 1637 990933-1 Liquids 25 42 24 50 0000 84 5 64-147 05/27/1999 1703 190933-2 Liquids 25 43 13 50 0000 86 3 64-147 05/27/1999 1729 90933-3 Liquids 5 46 78 50 0000 93 6 64-147 05/27/1999 1755 90933-7 Liquids 25 43 29 50 0000 86 6 64-147 05/27/1999 1913 990933-4 Liquids 1 48 32 50 0000 96 6 64-147 05/27/1999 2122 990905-2 Liquids 50 44 75 50 0000 89 5 64-147 05/27/1999 2148 90905-3 Liquids 1 49 86 50 0000 99 7 64-147 05/27/1999 2214 906-4 Liquids 50 43 66 50 0000 87 3 64-147 05/27/1999 2240 :1-1 liquids 1 43 58 50 0000 87 2 64-147 05/27/1999 2306 42-3 Solid 1 51 89 50 0000 103 8 64 147 05/27/1999 2332 90942-4 Solid 1 91 85 50 0000 183 7 64-147 X 05/27/1999 2358 Page 11