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COULAB CORE LABORATORIES <br /> S U R R 0 G A T E R E C O V E R I E S R E P O R T <br /> Job Number 990931 Report Date 05/31/1999 <br /> CUSTOMER IT Group PROJECT Southland - Martinez ATTN Bob Butter <br /> Surrogate Units <br /> 4-Bromofiuorobenzene ug/L <br /> Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time <br /> 990942-5 Solid 1 47 72 50 0000 95 4 64-147 05/28/1999 0024 <br /> Method Volatile Orgam cs by GC/MS Batch 6485 <br /> Method Code 8260OX Analyst vz <br /> —Surro_g_ate units <br /> Dthromofluoromethane ug/L <br /> Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time <br /> 881-3 Liquids 1 30 04 25 000 120 2 79-132 05/25/1999 1102 <br /> 81-3 Liquids MS 27 33 25 000 109 3 79-132 05/25/1999 1130 <br /> on 81-3 Liquids MSD 29 31 25 000 117 2 79-132 05/25/1999 1159 <br /> LCS 28 61 25 000 114 4 79-132 05/28/1999 1809 <br /> MB 28 43 25 000 113 7 79-132 05/28/1999 1837 <br /> 990931-2 Liquids 1 29 70 25 000 118 8 79-132 05/28/1999 1905 <br /> 1990931-2 Liquids MS 30 25 25 000 121 0 79-132 05/28/1999 1934 <br /> 990931-2 Liquids MSD 29 96 25 000 119 8 79-132 05/28/1999 2002 <br /> 990931-1 Liquids 20 30 34 25 000 121 4 79-132 05/28/1999 2031 <br /> 990931-3 Liquids 1 28 38 25 000 113 5 79-132 05/28/1999 2059 <br /> 990931-4 Liquids 1 29 34 25 000 117 4 79-132 05/28/1999 2127 <br /> 990932-1 Liquids 1 29 99 25 000 120 0 79-132 05/28/1999 2156 <br /> 990932-2 Liquids 1 27 40 25 000 109 6 79-132 05/28/1999 2224 <br /> 990932-3 Liquids 20 30 84 25 000 123 4 79-132 05/28/1999 2253 <br /> 990932-4 Liquids 50 29 23 25 000 116 9 79-132 05/28/1999 2321 <br /> 90933-1 Liquids 50 28 39 25 000 113 6 79-132 05/29/1999 0018 <br /> 990933-2 Liquids 10 25 86 25 000 103 4 79-132 05/29/1999 0047 <br /> 990933-3 Liquids 10 28 94 25 000 115 8 79-132 05/29/1999 0115 <br /> 990933-4 Liquids 1 26 61 25 000 106 4 79-132 05/29/1999 0144 <br /> F90933-5 Liquids 100 23 63 25 000 94 5 79-132 05/29/1999 0212 <br /> 0933-6 Liquids 1 22 50 25 000 90 0 79-132 05/29/1999 0241 <br /> 0933-7 Liquids 10 24 11 25 000 96 4 79-132 05/29/1999 0309 <br /> 990933-8 Liquids 2 23 83 25 000 95 3 79-132 05/29/1999 0338 <br /> 990932-5 Liquids 5 22 99 25 000 92 0 79-132 05/29/1999 0406 <br /> ' Page 12 <br /> , <br /> Nh <br /> ,n <br />