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' Alpha Analytical, Inc. <br /> 255 Glendale Ave •Suite 21 • Sparks, Nevada 89431-5778 <br /> (775)355-1044 •(775) 355-0406 FAX • 1-800-283-1183 <br /> Date <br /> 16 Na&,O? QC Summary Report Work Order <br /> 04102243 <br /> Method <br /> Method Blank Type MBLK Test Code SM3500-Fe D <br /> File ID Batch tD W041104FED Analysts Date 11/04/2004 00 00 <br /> Sample 10 MBLK-W041104FED Units mg1L Run ID WETLAB_041104E Prep Date 1110412004 <br /> Analyle Result PCIL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPDRefVal %RPD(Limit)Qua$ <br /> Iron Dissolved ND 03 <br /> Laboratory Control Spike Type LCS Test Code SM3500-Fe D <br />' File 10 Batch ID W041104FED Analysts Date 11104120040000 <br /> Sample ID LCS-W041104FED Units mg1L Run ID WETLAB_041104E Prep Date 11/04/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowUmtt Highl-imit RPDRefVaf %RPD(Limit) Qual <br />' Iron Dissolved 152 0 3 1 5 101 85 115 <br /> Sample Matrix Spike Type MS Test Code S&13500-Fe D <br /> File ID Batch ID W041104FED Analysts Date 11104/2004 00 00 <br /> Sample ID 04102701-02AMS Units mg/t. Run ID WETLAB_041104E Prep Date 11/04/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowtimit Highl-imit RPDRefVal %RPD(Limit) Qual <br /> Iron Dissolved 4 7 0 3 75 0 63 70 130 M2 <br /> Sample Matrix Spike Duplicate Type MSD Test Code SM3500-Fe D <br /> File ID Batch ID W041104FED Analysis Date 11/04/2004 00 00 <br /> Sample ID 04102701-02AMSD Units mg/L Run ID WETLAI3_041104E Prep Date 11/04/2004 <br />' Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Highl-imit RPDRefVal %RPD(Limit) Qual <br /> Iron Dissolved 5 0 3 75 0 67 70 130 4 7 6 2(20) M2 <br /> Comtnents <br /> Calculations are based oft'of raw(non rounded)data However for reporting purposes all QC data is rounded to three significant figures Therefore hand Lalculated <br /> values may differ slightly <br /> M2=Matrix spike recovery was low the inethod control sample recovery was acceptable <br /> r <br /> r <br /> r <br /> r <br /> r <br /> r <br /> r <br /> 1 I <br /> i <br /> r <br />