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Alpha Analytical, Inc. <br /> 255 Glendale Ave •Suite 21 •Sparks,Nevada 89431-5778 <br /> (775)355-1044 • (775)355-0406 FAX• 1-800-283-1183 <br /> Rare <br /> 16-Nov-04 QC Summary Report Work Order <br /> 04(02243 <br /> Method Blank Type MIOLK Test Code SM3500-Fe D <br /> File 1D Batch ID W041104FET Analysis pate 11/04/20040000 <br /> Sample ID MBLK-W041104FET Units mg1L Run ID WETLAB 041104D Prep Date 1110412004 <br /> Analyte Result PQL SpkVai SpkRefVal %REC LowUmit Hight mit RPDRefVai %RPD(Limit) Qual <br /> Iron Total ND 03 <br /> Laboratory Control Spike Type LCS Test Code SM3500-Fe D <br />' File ID Batch ID W041104FET Analysis Date 11104/2004 00 00 <br /> Sample ID LCS-W041104FET Units mg1L Run ID WETLAB_041104D Prep Date 1110412004 <br /> Analyte Result PQL SpkVat SpkRefVal %REC LowLemit Hrghl-imit RPDRefVat %RPD(Limt) Qual <br />' Iron Total 47 03 50 94 85 115 <br /> Sample Matrix Spike Type MS Test Code SM3500-Fe D <br /> File ID Batch ID W041104FET Analysis Date 11/04/2004 00 00 <br /> Sample ID 04102243-01AMS Units mglL Run ID WETLA8_041104D Prep Date 11/0412004 <br /> Analyte Result PQL SpkVat SpkRefVal %REC Lowl-imtt HighLimit RPDRefVal %RPD(Ltmit) Qual <br /> Iron Total 38 03 75 0 51 70 130 M2 <br /> Sample Matrix Spike Duplicate Type MSD Test Cade SM3500-Fe D <br /> File ID Batch ID W041104FET Analysis Date 1110412004 00 00 <br /> Sample ID 04102243-01AMSD Units mglL Run ID WETLA13_041104D Prep Date 1110412004 <br /> Analyte Result PQL SpkVat SpkRefVat %REC Lowl-imit HtghLimit RPDRefVa1 %RPD(Limit) Qual <br /> Iron Total 1 03 75 0 13 70 130 38 117 0(20) M2 <br /> R58 <br /> Comments <br /> Calculations are based off of raw(non rounded)data However for reporting purposes all QC data is rounded to three sigmtie-ant figures Theretore hand calculated <br /> values may differ slightly <br /> M2=Mitnx spike recovery was low,the method control sample recovery was acceptable <br /> R58=M&N1SD RPD exceeded the laboratory control limit <br /> 1 <br /> 1 <br />