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COLUMBIA ANALYTICAL SERVICES, INC. <br /> Analytical Report <br /> . Client: EMCON Service Request: S9901003 <br /> Project: Teichert&Sons-Stockton/20F90-002.007 Date Collected: 3/23/99 <br /> Sample Matrix: Soil Date Received: 3/25/99 <br /> Fuel Oxygenates <br /> Sample Name: SP-2A/B Units: ug/Kg(ppb) <br /> Lab Code: S9901001-026 Basis: Wet <br /> Test Notes: <br /> Prep Analysis Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> lert-Butyl Alcohol NONE 8260 500 1 4/2/99 4/2199 ND <br /> Methyl lert-Butyl Ether NONE 8260 5 1 4/2199 4/2/99 ND <br /> Diisopropyl Ether NONE 8260 50 1 4/2/99 4/2/99 ND <br /> Ethyl Cert-Butyl Ether NONE 8260 50 1 4/2/99 4/2/99 ND <br /> ter!-Amyl Methyl Ether NONE 8260 50 1 4/2/99 4/2199 ND <br /> iarwvc usp <br /> Page 4 <br />