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COLUMBIA ANALYTICAL SERVICES,INC. <br /> Analytical Report <br /> Client: EMCON Service Request: S9901001 <br /> Project: Teichert&Sons-Stockton/20F90-002.007 Date Collected: 3/23/99 <br /> Sample Matrix: Soil Date Received: 3/25/99 <br /> Fuel Oxygenates <br /> Sample Name.: SP-3AB Units: ug/Kg(ppb) <br /> Lab Code: S9901001-027 Basis: Wet <br /> Test Notes: <br /> Prep Analysis Dilution Date Date Result <br /> Analyte Method Method MRL Factor Extracted Analyzed Result Notes <br /> Cert-Butyl Alcohol NONE 8260 500 1 4/2/99 4/2/99 ND <br /> Methyl tert-Butyl Ether NONE 8260 5 1 4/2/99 4/2/99 ND <br /> Diisopropyl Ether NONE 8260 50 1 4/2199 4/2/99 ND <br /> Ethyl lert-Butyl Ether NONE 8260 50 1 4/2/99 4/2/99 ND <br /> cert-Amyl Methyl Ether NONE 8260 50 1 4/2/99 4/2/99 ND <br /> iarw�c �ry <br /> Page 5 <br />