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Alpha Analytical, Inc. <br /> 255 Glendale Ave • Suite 21 • Sparks,Nevada 89431-5778 <br /> (775)355-1044 • (775)355-0406 FAX• 1-800-283-1183 <br /> Date <br /> ork Order <br /> 15-Sep-04 QC Summary Report 0409082222 <br /> 04090 <br /> Method Blank Type MBLK Test Code EPA Method SW8015B/DHS LOFT Manual <br /> File ID D1HPCHEMIMS081DATA1040909104090905 D Batch ID MS08WO909B Analysis Date 09/09/2004 12 13 <br /> Sample ID MBLK MSOSWO909B Units p9/L Run ID MSD 08_040909A Prep Date 09/09/2004 <br /> Analyte Result POL SpkVal SpkRefVal %REC LowLimit Highl.imit RPDRefVal %RPD(Limit) Qua] <br /> TPH Purqeable ND 50 <br /> Surr 1,2-Dichloroethane-d4 931 10 93 72 126 <br /> Surr Toluene-dB 987 10 99 71 128 <br /> Surr 4-Bromofluorobenzene 105 10 105 76 121 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW801513/131-IS LUFT Manual <br /> Fife ID D 1HPCHEMIMS081DATA1040909104090904 D Batch ID MS08WO909B Analysis Date 09/09/200411 51 <br /> Sample ID GLCS MSOSWO909B Units pg/L Run ID MSD_08 040909A Prep Date 09/09/2004 <br /> Analyte Result POL SpkVal SpkRefVal %REC Lowtimit Highl-imit RPDRefVal %RPD(Limit) Qual <br /> TPH Purqeable 434 5o 400 108 67 136 <br /> Surr 1,2-Dichloroethane-d4 962 10 96 72 126 <br /> Surr Toluene-dB 894 10 89 71 128 <br /> Surr 4-Bromofluorobenzene 101 10 101 76 121 <br /> Sample Matnx Spike Type MS Test Code EPA Method SW8015B/DHS LUFT Manual <br /> File ID D 1HPCHEMIMS081DATA1040909104090912 D Batch ID MS08W0909B Analysis Date 09/091200414 46 <br /> Sample ID 04090340-OIAGS Units pg/L Run ID MSD_08_040909A Prep Date 09/09/2004 <br /> Analyte Result POL SpkVal SpkRefVal %REC LowUmit HighVmtt RPDRefVal %RPD(Umit) Qual <br /> TPH Purqeable 1880 250 2000 0 94 54 154 <br /> Surr 1,2-Dichloroethane-d4 41 2 50 82 72 126 <br /> Surr Toluene-d8 474 50 95 71 128 <br /> AMILurr_4-Bromofluorobenzene 512 50 102 76 121 <br /> ample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8015B/DHS LUFT Manual <br /> File ID D 1HPCHEMIMSOMDATA1040909104090913 D Batch ID MSOBWO909B Analysis Date 09/09/2004 15 08 <br /> Sample ID 04090340-01AGSD Units ttg/L Run ID MSD 08_040909A Prep Date 09/0912004 <br /> Analyte Result POL SpkVal SpkRefVal %REC LowLjmd Htghlimit RPDRefVal %RPD(Limit) Qual <br /> TPH Purqeable 1970 250 2000 0 98 54 154 1882 4 5(66) - <br /> Surr 1,2-Dichloroethane-d4 424 50 85 72 126 <br /> Surr Toluene-d8 47 50 94 71 128 <br /> Surr 4-Bromofluorobenzene 494 50 99 76 121 <br /> Comments <br /> Calculations are based off of raw(non-rounded)data However,for reporting purposes,all QC data is rounded to three significant figures Therefore,hand calculated <br /> values may differ slightly <br /> Reported in micrograms per hter,per client request <br />