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Alpha Analytical Inc. <br /> 255 Glendale Ave - Suite 21 - Sparks,Nevada 89431-5778 <br /> (775)355-1044- (775)355-0406 FAX- 1-800-283-1183 <br /> ate Work Order <br /> 5 Sep-04 QC Summary Report 04090822 <br /> Method Blank Type MBLK Test Code EPA Method SW8260B <br /> File ID D 1HPCHEM1MS081DATA1040909104090905 D Batch ID MSOSWO909A Analysis Date 09/09/2004 12 13 <br /> Sample ID MBLK MSOBWO909A Units pg/L Run ID MSD_08 040909A Prep Date 09/09/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighUmit RPDRefVal %RPD(L.imit) Qual <br /> Tertiary Butyl Alcohol (TBA) ND 10 <br /> Methyl tert butyl ether(MTBE) NO 0 5 <br /> Di-isopropyl Ether(DIPS) NO 1 <br /> Ethyl Tertiary Butyl Ether(ETBE) NO 1 <br /> 1 2-Dichloroethane NO 1 <br /> Benzene NO 05 <br /> Tertiary Amyl Methyl Ether(TAME) ND 1 <br /> Toluene NO 05 <br /> 1 2-Dibromoethane(EDB) NO 2 <br /> Ethylbenzene NO 0 5 <br /> m,p-Xylene NO 0 5 <br /> o-Xylene NO 05 <br /> Surr 1,2-Dichloroethane-d4 9 31 10 93 72 126 <br /> Surr Toluene-d8 987 10 99 71 128 <br /> Surr 4-Bromofluorobenzene 105 10 105 76 121 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW8260B <br /> File ID D 1HPCHEM1MS081DATA1040909104090903 D Batch ID MS08WO909A Analysis Date 09/09/2004 11 30 <br /> Sample ID LCS MSOSWO909A Units pg/L Run ID MSD_08_040909A Prep Date 09/09/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit Highl-imit RPDRefVal %RPD(L.imit) Qual <br /> Benzene 893 0 5 10 89 83 119 <br /> Toluene 898 0 5 10 90 80 120 <br /> wpVIbenzene 995 0 5 10 100 80 120 <br /> -Xylene 10 0 5 10 100 77 125 <br /> 9 81 0 5 10 98 77 124 <br /> Surr 1 2-Dichloroethane-d4 10 10 100 72 126 <br /> Surr Toluene-d8 981 10 98 71 128 <br /> Surr 4-Bromofluorobenzene 9 87 10 99 76 121 <br /> Sample Matrix Spike Type MS Test Code EPA Method SW8260B <br /> File ID D 1HPCHEM1MS081DATA1040909104090910 D Batch ID MSOSW09NA Analysts Date 09/09/2004 14 02 <br /> Sample ID 04090340-01AMS Units pg/L Run ID MSD 08 040909A Prep Date 09/09/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighUmit RPDRefVal %RPD(Umit) Qual <br /> Benzene 457 1 3 50 0 91 59 145 <br /> Toluene 464 1 3 50 0 93 39 161 <br /> Ethylbenzene 491 13 50 0 98 57 145 <br /> m,p-Xylene 505 1 3 50 0 101 37 163 <br /> o-XVlene 49 6 1 3 50 0 99 47 156 <br /> Surr 1,2-Dichloroethane-d4 422 50 84 72 126 <br /> Surr Toluene-d8 502 50 100 71 128 <br /> Surr 4-Bromofluorobenzene 507 50 101 76 121 <br /> Sample Matrix Spike Duplicate Type MSD Test Code EPA Method SW8260B <br /> File ID D IHPCHEM\MS081DATA1040909104090911 D Batch ID MSOSWO909A Analysis Date 09/09/2004 14 24 <br /> Sample ID D4090340-01AMSO Units pg/L Run ID MSD_08 040909A Prep Date 09/09/2004 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimrt Hlghl-imit RPDRefVal %RPD(Limd) Qual <br /> Benzene 461 1 3 50 0 92 59 145 45 67 1 0(22) <br /> Toluene 453 1 3 50 0 91 39 161 4644 2 6(22) <br /> Ethylbenzene 468 1 3 50 0 94 57 145 4907 4 8(22) <br /> m,p-Xylene 485 1 3 50 0 97 37 163 5052 4 1(23) <br /> o-Xylene 482 1 3 50 0 96 47 156 4961 2 8(50) <br /> Surr 1 2-Dichloroethane-d4 414 50 83 72 126 <br /> Surr Toluene-d8 483 50 97 71 128 <br /> rr 4-Bromofluorobenzene 506 50 101 76 121 <br />