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110 Second Avenue South,#fD7,Pacheco,CA 94553 <br /> 124 McCAMPBELL ANALYTICAL INC Telephone 510-798-1620 Fax 510-798-1622 <br /> http//,wwwmccam1)bellconi E-mail main@mccampbellcom <br /> • <br /> Advanced GeoEnvironmental Client Protect ID Den's Auto Date Sampled 09/08-09/11/97 <br /> 1803 West March Lane, Ste A Date Received 09/13/97 <br /> Stockton, CA 95207 Client Contact Bill Little Date Extracted 09/15/97 <br /> Client P O Date Analyzed 09115-09/16/97 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 80768 <br /> Client ID B4-85 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br />' Acetone ND trans-l,3-Dich)oropropene ND <br /> Benzene ND Ethylene dibromide' ' ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochloromethane ND Hexachlorobuiadiene ND <br /> Bromodichloromethane ND lodomethane ND <br /> Bromoform ND Isopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone"' ND <br />' sec-Butyl benzene ND Methylene Chloride" ND <br /> cert-Butyl benzene ND Methyl ethyl kelone'K' ND <br /> Carbon Disulfide ND Methyl isobutyl ketone` ' ND <br /> Carbon Tetrachloride ND Methyl tert Butyl Ether(M FB E) --- <br />'. Chlorobenzene ND Napthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether` ND Styrene" I ND <br /> Chloroform ND 1 112-Teti achloioethane ND <br /> Chloromethane ND 1,1,2,2 Tetrachloroethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene"" ND <br /> Dibromochloromethane ND 1,2 3 Tiichloiobenzene ND <br /> I 1,2-Dibromo-3-chloropropane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND 1,1 1-Tnchloroethane ND <br /> 1,2-Dichlorobenzene ND 1 1,2 Trichloroethane ND <br /> 1,3-Dichlorobenzene ND Trichloroethene ND <br /> 14-Dichlorobenzene ND Tnchlorofluolomet}iane ND <br /> Dichlorodtfluoromethane ND 1 2,3 Trichloropropane ND <br /> 1,1-Dichloroethane ND 1,24-Trimethylbenzene ND <br /> 1,2-Dichloroethane ND 1,3,5-Trimethyl benzene ND <br /> LI-Dichloroethene ND Vinyl Acetate"" ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride"' ND <br /> tr2ns-1,2-Dichloroethene ND Xylenes total " ND <br /> 1,2-Dichloropropane ND Comments <br /> 1,3-Dichloropropane ND Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND Dibromofluoromethane 96 <br /> I,1-Dichloropropene ND I Toluene-d8 105 <br /> cis-1,3-Dichloropropene ND 4 Bromofluorobenzene 96 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,vs ipes in ug/a ipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L N apor samples 0 5 ug/L,solid and sludge samples 5 ug/kg,wipes 0 2ug/w1pe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> . pentanone or isopropylacetone, (h) lighter than water immiscible sheen is piesent (i) liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (h) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />