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110 Second Avenue South,#D7,Pacheco,CA 94553 <br /> 4 MCCAMPBELL ANALYTICAL INC Telephone 510-798-1620 Fax 510-798-1622 <br /> h=//wAw mccamobell com E-mail main@mccampbell com <br /> Advanced GeoEnvironrnental Client Project ID Den's Auto Date Sampled 09/08-09/11/97 <br /> 1803 West March Lane, Ste A Date Received 09/13/97 <br />' Stockton, CA 95207 Client Contact Bill Little Date Extracted 09/15/97 <br /> Client P O Date Analyzed 09/15-09/16197 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br />' Lab ID 80771 <br /> Client ID B5-15/14 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br />' Acetone ND<200 trans-1,3-Dichloropropene 246X100 <br /> Benzene ND<100 Ethylene dibromide` ' ND<100 <br /> Bromobenzene ND<100 Ethylbenzene 1200 <br /> Bromochloromethane ND<100 Hexachlorobutadiene ND<100 <br />' Bromodichloromethane ND<100 Iodomethane ND<100 <br /> Bromoform NIX 100 Isopropylbenzene 3600 <br /> Bromomethane ND<300 p-Isopropyl toluene ND<100 <br /> n-Butyl benzene 12,000 Methyl butyl ketone"' ND<100 <br /> sec-Butyl benzene 2100 Methylene Chloride" ND<1Q0 <br /> tent-Butyl benzene 2000 Methyl ethyl ketones' ND<100 <br /> Carbon Disulfide ND<100 Methyl isobutyl ketone ' ND<100 <br /> Carbon Tetrachloride ND<100 Methyl tert-But)I Ether(MTBE) --- <br /> Chlorobenzene ND<100 Napthalene 1300 <br /> Chloroethane ND<100 n-Propyl benzene 11,000 <br /> 2-Chloroethyl Vinyl Ethe ND<100 Srvrene"' N13<100 <br /> Chloroform NLX 100 1,1 1 2-Tetrachloroetliane ND<100 <br /> Chloromethane ND<100 1 J,2 2-Tetrachloroethane ND<100 <br /> 2-Chlorotoluene ND<100 Tetrachloroethene ND<100 <br /> 4-Chlorotoluene ND<100 Toluene "' 220 <br />' Dibromochloromethane ND<100 1.2 3-Trichlorobenzene ND<100 <br /> 12-Dibromo-3-chloropropane ND<100 12,4-Tnchlorobenzene ND<100 <br /> Dibromomethane ND<100 1,1,1 Trichloroethane ND<100 <br /> 1,2-Dichlorobenzene ND<100 1 1 2-Tri chloroethane ND<100 <br />' 1,3-D,3ND<100 Trichloroethene ND<100 <br /> 1,4-Dichlorobenzene ND<100 Tnehlorofluoromethane ND<100 <br /> Dichlorodifluoromethane ND<100 1 2 3-Trichloropropane ND<100 <br /> FI-Dichloroethane ND<100 1,2 4-Trimeihylbenzene 82,000 <br /> 1,2-Dichloroethane ND<100 1,3,5-Trimethylbenzene 19 000 <br /> 1,1-Dichloroethene ND<100 Vmyl Acetate'"' ND<100 <br /> cis-1,2-Dichloroethene ND<100 Vinyl Chloride"' ND<100 <br /> trans 1,2-Dichloroethene ND<100 A)lenes total 'P' 71,000 <br /> 12-Dichloropropane N5X100 Comments <br /> 1,3-Dichloropropane ND<100 S u i rogate Reco-series(%) <br /> 2,2-Dichloropropane ND<100 Dibromofluoiomethane 104 <br /> 11-Dichloropropene ND<100 Toluene-d8 99 <br /> cis-1,3 Dichloropropene ND<100 4-Bromofluorobenzene 90 <br /> Nater and vapor samples are reported in ug/L,soil and sludge samples m ug/kg,i%apes in ug/N ipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples I ug/L,%apor samples 0 5 ug/L solid and sludge samples 5 ug/kg,Napes 0 2ug/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropytacetone, (h)lighter than water immiscible sheen is piesent (i) liquid sample that contains greater than —5 vol % <br /> I sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene (m) acetic acid etbenyl ester (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 //'l Edward Hamilton, Lab Director <br />