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110 Second Avenue South,#137,Pacheco,CA 94553 <br />' 4 1 McCAMPBELL ANALYTICAL INC Telephone 510-798-1620 Fax 510-798-1622 <br /> http//www mccampbell com E-mail main@mccampbell com <br />' Advanced GeoEnvironmental Client Protect ID Den's Auto Date Sampled 09/08-09/11/97 <br />' 1803 West March Lane, Ste A <br /> Date Received 09/13/97 <br /> Stockton, CA 95207 Client Contact Bill Little Date Extracted 09/15/97 <br />' Client P O Date Analyzed 09/15-09/16/97 <br /> Volatile Organics By GCIMS <br /> EPA method 8260 <br />' Lab ID 80773 <br /> Client ID BS-50 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> AcetoneNO trans-1,3-Dichloropropene NO <br /> Benzene NO Ethylene dibromide' ' NO <br /> Bromobenzene ND Ethytbenzene NO <br /> Bromochloromethane NO Hexachlorobutadiene NO <br />' Bromodichloromethane NO lodomethane NO <br /> Bromoform NO Isopropylbenzene NO <br /> Bromomethane ND p-lsopropyl toluene NO <br /> n-Butyl benzene NO Methyl butyl ketone"' NO <br />' sec-Butyl benzene NO Methylene Chloride'' ND <br /> tert-Butyl benzene ND Methyl ethyl ketone"' ND <br /> Carbon Disulfide ND<10 Methyl isobutyl ketone' ' NO <br /> Carbon Tetrachlonde NO Methyl tert-Butyl Ether(MTBE) -- <br /> Chlorobenzene NO Napthalene NO <br /> Chloroethane NO n-Propyl benzene NO <br /> 2-Chiorocthyt Vinyl Ether` NO styrene'liND <br /> Chloroform ND 1,1,1,2-Tetrachloroethane NO <br /> Chloromethane NO 1,1,2,2-Tetrachloroethane NO <br /> 2-Chlorotoluene ND Tetrachloroethene NO <br /> 4-Chlorotoluene NO Toluene"" NO <br /> Dibromochloromethane NO 1 2 3-Tnchlorobenzene ND <br /> 1,2-Dibmmo-3-chloropropane NO 1,2,4-Trichlorobenzene ND <br /> Dibromomethane NO 1 €,1-Trichloroethane NO <br /> 1,2-Dichlorobenzene NO 1,1,2-Trichloroethane ND <br /> 3,3-Dichlorobenzene NO Trichloroethene NO <br /> 14-Dichlorobenzene NO Trichlorofluoromethane NO <br /> Dichlorodifluoromethane ND 1 2 3-Trichloropropane NO <br /> 1,1-Dichloroethane ND 12,4-Tnmethylbenzene NO <br /> 1 2-Diebloroethane NO 7_35 5 TrimethyIbenzene 12 <br /> 1,1-Dichioroethene NO Vinyl Acetate"" NO <br /> cis-1,2-Dichloroethene NO Vinyl Chloride`°' NO <br /> trans-1,2-Dichloroethene NO Xylenes total 'a 14 <br /> 1,2-Dichloropropane ND Comments <br /> 1,3-Dichloropropane ND Surrogate Reco%eries(%} <br /> 2,2-Dichloropropane ND Dibromolluoromethane 100 <br /> 17l-Dichlmopropene ND Toluene-d8 103 <br /> cis-1,3-Dichloropropene ND I 4-Bromofluorobenzene 94 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg a ipes in ug/wipe and all TCLP I SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples I ug/L N apor samples 0 5 ug/L solid and sludge samples 5 ug/kg, Aipes 0 2ug/wipe <br /> ND means not detected above the reporting hrrat,N/A means analyte not apphcable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone (e) dichloiomethane (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone (h)lighter than water immiscible sheen is present (1) liquid sample that contains greater than--5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (€) methylbenzene (m) acetic acid ethenyl ester, (n) <br /> chloraethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 // Edward Hamilton, Lab Director <br />