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110 Second Avenue South,##D7,Pacheco,CA 94553 <br /> MCCAMPBELL ANALYTICAL INC Telephone 510-798-1620 Fax 510-798-1622 <br /> i 24 httn llwww mccampbell com E-mail main@mccampbell corn <br /> Advanced GeoEnvironmental Client Project ID Den's Auto Date Sampled 09/08-09/11/97 <br />' 1$03 West March Lane, Ste A <br /> Date Received 09/13/97 <br /> Stockton, CA 95207 Client Contact Bill Little Date Extracted 09/15/97 <br />' Client P O Date Analyzed 09/15-09/16/97 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br />' Lab ID 80772 <br /> Client ID B5-35 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND trans-1,3-Dichloropropene ND <br /> Benzene ND Ethylene dibromide' ' ND <br /> Bromobenzene ND Ethylbenzene ND <br /> Bromochloromethane ND Hexachlorobutadiene ND <br /> Bromodichloromethane ND lodomethane ND <br /> Bromoform ND Isopropylbenzene ND <br /> Bromomethane ND p-Isopropyl toluene ND <br /> n-Butyl benzene ND Methyl butyl ketone"' ND <br /> sec-Butyl benzene ND Methylene Chloride"' ND <br /> tent-Butyl benzene ND Methyl ethyl ketone'x' ND <br /> Carbon Disulfide ND Methyl isobutyl ketone' ' <br /> Carbon Tetrachloride ND Methyi tert-Butyl Ether(MTBE) ND <br /> Chlorobenzene ND Napthalene ND <br /> Chloroethane ND n-Propyl benzene ND <br /> 2-Chloroethyl Vinyl Ether` ND Styrene" ND <br /> Chloroform ND 1 11,2-Tetrachloroethane ND <br /> Chloromethane ND 1,1,2 2-Tetrachloioethane ND <br /> 2-Chlorotoluene ND Tetrachloroethene ND <br /> 4-Chlorotoluene ND Toluene"" ND <br /> Dibromochloromethane ND 1,2,3 Tnchlorobenzene ND <br />' 1,2-Dibromo-3-chloropropane ND 1,2,4-Trichlorobenzene ND <br /> Dibromomethane ND 1,11-Trichloroethane ND <br /> 1,2-Dichlorobenzene ND 1,1,2-Trichloroethane ND <br /> 1,3-Dichlorobenzene ND Tnchloioethene ND <br /> 1,4-Dichlorobenzene ND Trichlorofluoromethane ND <br /> Dichlorodifluoromethane ND 1,2 3-Trichloropropane ND <br /> 1,1-Dichloroethane ND 12,4-Tnmethylbenzene ND <br /> 1,2-Dichloroethane ND 1,3,5-Trimeihylbenzene ND <br /> l,1-Di chloroethene ND Vinyl Acetate"" ND <br /> cis-1,2-Dichloroethene ND Vinyl Chloride'°' ND <br /> tr2ns-1,2-Dichloroethene ND Xylenes total 'p' ND <br /> 1,2-Dichloropropane ND Comments <br /> 1,3-Dichloropropane ND Surrogate Reco.eries(%) <br /> f2-Dichloropropane ND DlbromofluOionlethane 102 <br /> l,l-Dichloropropene ND Toluene-d8 106 <br />' cis-1,3-Dichloropropene ND 4-Bromofluorobenzene 96 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in uglkz, wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L vapor samples 0 5 ug/L solid and sludge samples 5 ug/kg wipes 0 2u&/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene, (d) 2-hexanone (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (i) liquid sample that contains greater than --5 vol % <br /> sediment, 0) sample diluted due to high organic content, (k) ethenylbenzene (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />