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19 January 2012 <br /> AGE-NC Project No. 11-2006 <br /> Page 3 of 7 <br /> • VOCs in accordance with EPA method 8260B; and <br /> • SVOC's in accordance with EPA method 8270. <br /> SOIL-VAPOR SAMPLE COLLECTION <br /> Soil-vapor samples were collected using a Geoprobe soil-vapor sampling assembly from <br /> borings V1 and V2 at depths of 5 feet bsg. An expendable vapor point was placed into a <br /> point holder at the bottom of an assembly of 1.25-inch diameter hollow rods.The assembly <br /> was then advanced to the specified depth (i.e. 5 feet bsg) and retracted approximately <br /> twelve inches in order to disengage the bottom expendable point and expose a column of <br /> strata from which soil-vapor could be extracted. Single use, '/4-inch diameter disposable <br /> polyethylene tubing was then attached to a tubing adapter equipped with an O-ring to <br /> ensure a vacuum-tight seal. The adapter assembly was lowered through the center of the <br /> hollow drive rods to the specified depth and secured by threading into the expendable <br /> vapor point holder. <br /> Above ground, the surface around the soil-vapor sampler was sealed with bentonite <br /> powder and hydrated to prevent ambient air intrusion. Soil- vapor sample collection was <br /> conducted using 1-liter Tedlar bags. To ensure that a reliable soil-vapor sample was <br /> collected with no ambient air breakthrough down the probe rod, AGE erected a plastic <br /> enclosure over the probe rod, and applied an appropriate amount (approximately 6 to 8 <br /> ounces) of Isopropyl Alcohol (IPA) as a tracer to adequately wet a towel; the wetted towel <br /> was completely wrapped around the base of the probe rod where it contacted the surface <br /> and the bentonite seal. <br /> The end of the polyethylene tubing was attached by a two-way inlet port to a Tedlar bag <br /> placed inside an SKC Vac-U-Chamber (lung box) vacuum chamber. A vacuum pump <br /> attached to a purge port of the vacuum chamber was then used to purge the exposed soil <br /> column, through the sampling tubing and inlet port, until at minimum, three volumes of <br /> soil-vapor and ambient air were evacuated through the sampling system. The vacuum <br /> chamber was sealed and the vacuum pump was then attached to the vacuum outlet port <br /> of the chamber. Vacuum was applied to the chamber to create negative pressure around <br /> the Tedlar bag, which inflated and allowed the soil-vapor sample to enter directly into the <br /> bag via the inlet port. When the sample was collected, the negative pressure in the <br /> chamber was reduced and the sample bag was sealed, labeled, logged on a chain of <br /> custody form, and placed into a dry cooler (room temperature). All of the collected <br /> soil-vapor samples were delivered to CTEL and analyzed for the following constituents: <br /> • TPH-g in accordance with EPA Modified Method TO-3; and <br /> • BTEX and Isopropyl alcohol (IPA)in accordance with EPA Modified Method TO-17. <br /> Advanced GeuEnvironmental,Inc. <br />