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110 Second Avenue South,##137,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> htto.1/www. cc m pbell.com E-mail:main @mccampbell.com <br /> ~ Date Sampled: 04/22/98 <br /> Advanced GeoEnvironmental Client Project ID: Stockton Plat <br /> Date Received: 04/24/98 <br /> 4005 North Wilson Way <br /> Stockton,CA 95205 Client Contact:Bill Little Date Extracted:04/24/98 <br /> Fieit <br /> PA: Date Analyzed: 04/24/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 88423 <br /> Client ID ASB7 <br /> Matrix W <br /> Compound Concentration* Compound Concentration" <br /> Acetone` ' ND<5 Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND <br /> Bromoform ND Methyl butyl ketone' ' ND <br /> Bromomethane ND Methylene Chloride" ND <br /> n-Butyl benzene ND Methyl ethyl ketone ND <br /> sec-Butyl benzene ND Methyl isobutyl ketones ND <br /> Cert-Butyl benzene ND Methyl ten-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND Napthaiene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND Styrene' ND <br /> Chloroethane ND 1,1,1,2-Tetrachloroethane ND <br /> 2-Chloroethyl Vinyl Ether` ND 1,1,2,2-Tetrachloroethane ND <br /> Chloroform ND Tetrachloroethene ND <br /> Chloromethane ND Toluene" ND <br /> 2-Chlorotoluene ND 1,2,3-Trichlorobenzene ND <br /> 4-Chlorotoluene ND 1,2,4-Trichlorobenzene ND <br /> Dibromochloromethane ND 1,1.1-Trichloroethane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Trichloroethane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Trichlorofluoromethane ND <br /> 1,3-Dichlorobenzene ND 1,2.3-Trichloropropane ND . <br /> 1,4-Dichlorobenzene ND 1,2,4-Trimethylbenzene ND <br /> Dichlorodifluoromethane ND 1,3.5-Trimethylbenzene ND <br /> 1,1-Dichloroethane ND Vinyl Acetate ND <br /> 1,2-Dichloroethane ND Vinyl Chloride ND <br /> ],1-Dichloroethene ND Xylenes,total ND <br /> cis-1,2-Dichloroethene ND <br /> trans-l,2-Dichloroethene ND <br /> 1,2-Dichloropropane ND <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments:i <br /> 1,1-Dichloropropene ND Surrogate Recoveries(°/„) <br /> cis-1,3-Dichloropropene 'ND Dibromoiluoromethane 86 <br /> trans-l,3-Dichioropropene ND Toluene-d8 102 <br /> Ethylene dibromide ND 4-Bromoiluorobenzene 104 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP.1 SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated: water samples 1.0 ug/L; vapor samples OS ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2ug/wipe ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone;(h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than —5 vol. % <br /> sediment;0)sample diluted due to high organic content;(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester,(n)chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 / Edward Hamilton,Lab Director <br /> 4 <br />