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I 10 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. . Telephone:925-798-1620 Fax:925-798-1622 <br /> hU://www.mccAmi2bell-co E-mail:main@mccampbell.com <br /> Date Sampled: 04/22/98 <br /> Advanced GeoEnvironmental Client Project ID: Stockton PIat <br /> 4005 North Wilson Way 'Date Received: 04/24/98 <br /> Stockton,CA 95205 Client Contact: Bill Little Date Extracted: 04/24/98 <br /> Client P.O: Date Analyzed: 04127-04128198 <br /> Volatile Organics By GUMS <br /> EPA method 8260 <br /> Lab ID 88426 <br /> Client ID ASB6-45 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone ' ND<100 Ethylbenzene 1700 <br /> Benzene 480 Hexachlorobuladiene ND<200 <br /> Bromobenzene ND<200 lodomethane ND<200 <br /> Bromochloromethane ND<200 isopropylbenzene 190 <br /> Bromodichloromethane ND<200 p-lsopropyl toluene ND<200 <br /> Bromoform ND<200 Methyl butyl ketone' ' ND<200 <br /> Bromomethane ND<200 Methylene Chloride" ND<200 <br /> n-Butyl benzene 380 Methyl ethyl ketone ' ND<800 <br /> sec-Butyl benzene ND<200 Methyl isobutyl ketone'x ND<200 <br /> tert-Butyl benzene 540 Methyl tert-Butyl Ether(MTBE) -- <br /> Carbon Disulfide ND<200 Naphthalene 340 <br /> Carbon Tetrachloride ND<200 n-Propyl benzene 740 <br /> Chlorobenzene ND<200 Styrene' ' ND<200 <br /> Chloroethane ND<200 1,1,l,2•Tetrachloroethane ND<200 <br /> 2-Chloroethyl Vinyl Ethe? NDC200 1,1.2,2-Tetrachloroethane ND<200 f <br /> Chloroform NDC200 Tetrachloroethene ND<200 <br /> Chloromethane NDC200 Toluene" 2500 <br /> 2-Chlorotoluene ND<200 1,2,3-Trichlorobenzene ND<200 <br /> 4-Chlorotoluene ND<200 1,2,4-Trichlorobenzene ND<200 <br /> Dibromochloromethane ND<200 1,1,1-Tri chloroethane ND<200 <br /> 1,2-Dibromo-3-chloropropane ND<200 1,1,2-Trichloroethane ND<200'. <br /> Dibromomethane ND<200 Trichloroethene ND<200 <br /> 1,2-Dichlorobenzene ND<200 Trichlorofluoromethane ND<200 <br /> 1,3-Dichlorobenzene ND<200 1,2,3-Trichloropropane NDc200 <br /> 1,4-Dichlorobenzene ND<200 1,2,4-Trimethylbenzene 4300 <br /> Dichlorodifluoromethane ND-C200 1,3,5-Trimethylbenzene 1400 <br /> ],I-Dichloroethane ND<200 Vinyl Acetate'"" 420 <br /> 1,2-Dichloroethane ND<200 Vinyl Chloride"" ND<200 <br /> I,l-Dichloroethene ND<200 Xylenes,total '°' 7300 <br /> cis-1,2-Dichloroethene ND<200 i <br /> trans-l,2-Dichloroethene ND<200 <br /> 1,2-Dichloropropane ND-5200 <br /> 1,3-Dichloropropane ND<200 <br /> 2,2-Dichloropropane ND<200 Comments: <br /> 1,1-Dichloropropene ND<200 Surrogate Recoveries{%) <br /> cis-1,3-Dichloropropene ND<200 Dibromofluoromethane 85 <br /> trans-1,3-Dichloropropene ND<200 Toluene-d8 101 <br /> Ethylene dibromide ND<200 4-Bromofluorobenzene 107 <br /> 'waier and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated: water samples 1.0 ug/L; vapor samples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2ug/wipe ND means not detected above the reporting limit;NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexanone; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone;(h)lighter than water immiscible sheen is present; (i)liquid sample that contains greater than —5 vol. % <br /> sediment;0)sample diluted due to high organic content;(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(t)methylbenzene;(m)acetic acid ethenyl ester;(n}chloroeihenc,(o)dimethylbenzenes. <br /> DHS Certification No. 1644 Edward Hamilton,Lab Director <br />