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819 Sinker Avenue Suite 8 <br /> TesU)�,merica Sacramento C 95834 <br /> (916)922 1-96%01] <br /> ANALYTICAL TESTING CORPORATION FAX(916) 0 <br /> www tcstamencamarnloo c con,om <br /> Blaine Tech Services(Shell) Project Shell 2320 N Eldorado,Stockton S607171 <br /> 1680 Rogers Avenue Project Number 97471966_SAP# 136145 Repo rtedw <br /> San Jose CA,95112 Project Manager Jason Bron 07/24/06 15 52 <br /> GasolmeMEMOxygenates by EPA method 8260B <br /> TestAmerlca - Sacramento, CA <br /> Reporting <br /> Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Note <br /> MW-1(5607171-01)Water Sampled 07/07/0613 10 Received 07/12/06 13 30 <br /> Ethanol ND 50 ug/1 1 6070218 07/19/06 07/20/06 EPA 8260B <br /> Tert-butyl alcohol 30 5 0 " <br /> Methyl tert-butyl etber ND 050 ^ <br /> Dt-isopropyl ether 74 20 " <br /> Ethyl tert-butyl ether ND 20 " <br /> Tert-amyl methyl ether ND 20 " <br /> Benzene 31 050 <br /> Ethylbenzene 83 050 " <br /> Toluene 12 050 " <br /> Xylenes(total) 77 10 " <br /> Gasoline Range Organics(C4-C12) 3600 50 <br /> Surrogate 1,2-DCA-d4 104% 60-140 " <br /> Surrogate Toluene-d8 101 % 60-140 " <br /> Surrogate 4-BFB 102% 60-140 " <br /> MW-2(S607171-02)Water Sampled 07/07/06 12 30 Received 07/12/06 13 30 <br /> Ethanol ND 50 ug/l 1 6070218 07/19/06 07/20/06 EPA 8260E <br /> Tert-butyl alcohol ND 5 0 " <br /> Methyl tert-butyl ether ND 050 " <br /> Di-isopropyl ether ND _ 2 0 " <br /> Ethyl tert-butyl ether ND 2 0 <br /> Tert-amyl methyl ether ND 2 0 <br /> Benzene ND 0 50 " <br /> Ethylbenzene ND 050 " <br /> Toluene ND 050 " <br /> Xylenes(total) ND 1 0 " <br /> Gasoline Range Organics(C4-C12) 480 50 <br /> Surrogate 12-DCA-d4 100% 60-140 " <br /> Surrogate Toluene-d8 100% 60-140 " <br /> Surrogate 4-BFB 102% 60-140 " <br /> TestAmerlca- Sacramento,CA The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document Unless otherwise stated results are reported on a wet weight basis <br /> This analytical report must be reproduced in its entirety <br /> Page 3 of 8 <br />