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819 Striker Avenue Suite 8 <br /> TesU�merica <br /> Sacramento, 92 95834 <br /> -9600(916)921-9600 <br /> FAX(916)921-0100 <br /> ANALYTICAL TESTING CORPORATION www testamencamc corn <br /> Blaine Tech Services(Shell) Project Shell 2320 N Eldorado,Stockton S607171 <br /> 1680 Rogers Avenue Project Number 97471966 SAP#136145 Reported <br /> San Jose CA,95112 Project Manager Jason Brown 07/24/06 15 52 <br /> Gasoline\BTEXIOxygenates by EPA method 8260B <br /> TestAmerica- Sacramento, CA <br /> Reporting <br /> Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Note <br /> MW-3(S607171-03)Water Sampled 07/07/06 12 00 Received 07/12/06 13 30 <br /> Ethanol ND 50 ug/l 1 6070218 07/19/06 07/20/06 EPA 8260B <br /> Tert-butyl alcohol ND 50 " <br /> Methyl tert-butyl ether 077 050 " <br /> Di-isopropyl ether ND 20 <br /> Ethyl tert-butyl ether ND 20 <br /> Tert-amyl methyl ether ND 20 " <br /> Surrogate 1,2-DCA-d4 102% 60-140 <br /> Surrogate Toluene-d8 98% 60-140 <br /> Surrogate 4-BFB 105% 60-140 <br /> MW4(S607171-04)Water Sampled 07/07/06 11 30 Received 07/12/06 13 30 <br /> Ethanol ND 50 ug/1 1 6070218 07/19/06 07/20/06 EPA 8260B <br /> Tert-butyl alcohol ND 50 " <br /> Methyl tert-butyl ether 63 050 " <br /> E Di-isopropyl ether ND 20 <br /> Ethyl tert-butyl ether ND 20 " <br /> Tert-amyl methyl ether ND 20 " <br /> Surrogate 12-DCA-d4 108% 60-140 <br /> Surrogate Toluene-d8 96% 60-140 " <br /> Surrogate 4-BFB 108% 60-140 " <br /> TestAmerica- Sacramento,CA The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document Unless otherwise stated results are reported on a wet weight bases <br /> This analytical report must be reproduced in its entirety <br /> Page 4 of 8 <br />