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S 19 Striker Avenue Suite S <br /> TestAmericaSacram(91 C 9(916)9219600 <br /> FAX(916)921 0100 <br /> ANALYTICAL TESTING CORPORATION WWW testamencameCon, <br /> i <br /> Blaine Tech Services(Shell) Project Shell 2320 N Eldorado,Stockton 5607171 <br /> 1680 Rogers Avenue Project Number 97471966 SAP# 136145 Reported <br /> San Jose CA,95112 Project Manager Jason Brown 07/24/06 15 52 <br /> Gasoline1BTEX\Oxygenates by EPA method 8260B- Quality Control <br /> TestAmerica - Sacramento, CA <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch 6070218-EPA 5030B 1P/T1/EPA 8260B <br /> Blank(6070218-BLKI) Prepared 07/19/06 Analyzed 07/20/06 ~ <br /> Ethanol ND 50 ug/l <br /> Tert-butyl alcohol ND 50 " <br /> Methyl tert-butyl ether ND 050 " <br /> Di-isopropyl ether ND 20 " <br /> Ethyl tert-butyl ether ND 20 " <br /> Tert-amyl methyl ether ND 20 " <br /> 1,2 Dichloroethane ND 050 " <br /> 1,2-Dibromoethane(EDB) ND 050 " <br /> Benzene ND 0 50 " <br /> Ethylbenzene ND 050 " <br /> Toluene ND 050 " <br /> Xylenes(total) ND 1 0 " <br /> Gasoline Range Organics(C4-C 12) ND 50 <br /> Surrogate 12-DCA-d4 101 100 101 60-140 <br /> Surrogate Toluene-d8 976 100 98 60-140 <br /> Surrogate 4-BFB 102 100 102 60-140 <br /> Blank(6070218-BLK2) Prepared&Analyzed 07/20/06 <br /> Ethanol ND 50 ugll <br /> Tert-butyl alcohol ND 50 " <br /> Methyl tert-butyl ether ND 050 " <br /> Dr-isopropyl ether ND 2 0 <br /> Ethyl tert-butyl ether ND 20 " <br /> Tert-amyl methyl ether ND 20 " <br /> 1,2-Dichloroethane ND 0 50 " <br /> 1,2-Dibromoethane(EDB) ND 050 " <br /> Benzene ND 050 " <br /> Ethylbenzene ND 050 " <br /> Toluene ND 0 50 <br /> Xylenes(tote[) ND 10 " <br /> Gasoline Range Organics(C4-C 12) ND 50 " <br /> i <br /> Surrogate 12-DCA-d4 103 100 103 60-140 <br /> Surrogate Toluene-d8 9 64 100 96 60-140 <br /> Surrogate 4-BFB 9 95 100 100 60-140 <br /> a <br /> TestAmenca- SaCranlento, CA The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document Unless otherwise stated results are reported on a wet weight basis <br /> This analytical report must be reproduced in its entirety <br /> Page 5 of 8 <br />