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i <br /> aa) Analytical Laboratory CERTIFICATE OF ANALYSIS <br /> Sunday,January 8,2006 <br /> Attention Jack Bishop <br /> California Tank Lines Report Page 18 of21 <br /> P 0 BOX 6245 <br /> Stockton,CA 95206 <br /> Volatile Organic Compounds by EPA Method 8260B-Quality Control <br /> Precision Enviro-Tech <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Umts Level Result %REC Limits RPD Limit Notes <br /> Batch AL52105-Volatiles <br /> Blank(ALS2105-BLKI) Prepared&Analyzed 21-Dec-05 <br /> Acetone ND 500 tmgfl <br /> tert Butyl Acohol(TBA) ND 500 " <br /> Methyl term butyl Ether(MtBE) ND 0 500 <br /> Dnsopropyl Ether(DIPE) ND 0 500 <br /> Ethyl tert-Bury]Ether(ETBE) ND 0 500 " <br /> tert Amyl Methyl Ether(TAME) ND 0 500 <br /> 1,2-Dibromoethane(EDB) ND 0 500 " <br /> l 2-Dichloroethane ND 0 500 " <br /> Benzene ND 0 500 " <br /> Ethylbenzene ND 0 500 " <br /> luene ND 0 500 <br /> Xylene ND 0 500 " <br /> 0-Xylene ND 0 500 " <br /> LCS(AL52105-BSI) Prepared&Analyzed 21-Dec-05 <br /> Benzene 502 0 500 ug/1 500 100 75-122 <br /> 1 1 Dichloroethene 551 500 Soo 110 74 136 <br /> Toluene 484 0 500 500 97 75 122 <br /> Chlorobenzene 506 500 500 101 89 124 <br /> Matrix Spike(AL52105-MSI) Source 5122114-02 Prepared 21-Dec-05 Analyzed 22-Dec-05 <br /> Benzene 504 0 500 U94 500 398 93 75-122 <br /> 1 1 Dichloroethene 541 500 500 620 96 74-136 <br /> Toluene 484 0 500 500 ISO 94 75-122 <br /> Chloroberime 475 500 500 139 92 89-124 <br /> Matnx Spike Dup(AL52105-MSDI) Source 5122114-02 Prepared 21-Dec-05 Analyzed 22-Dec-05 <br /> Benzene 44 1 0 500 u811 50 0 388 80 75-122 13 15 <br /> 1 1-Drchlomethcne 46 6 500 50 0 620 81 74 136 15 20 <br /> Toluene 42 5 0 500 50 0 150 82 75 122 13 15 <br /> Chlorobenzene 43 4 500 500 139 84 70-124 9 20 <br /> mg/L=mdhgrams per b =ppm DLR-Derecnoa bma for purpose ofReporrrng <br /> ug/L-mrcmgmmrs per Luer-ppb F. cepa mal sample marnces or mierf renew may <br /> result rn higher detecnon limits <br /> RESPECTFULLY SUBMITTED, <br /> Jonathan L.egLqkpratory Director <br /> 7 743 N Nest Lane Suite 132 Stockton CA 95210 nhone (209) 477-8105 Fax (209) 477-8148 <br /> I <br /> I <br />