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- Analytical Laboratory CERTIFICATE OFANAL YSIS <br /> Sunday,January 8,2006 <br /> Attention Jack Bishop <br /> California Tank Lines <br /> Report Page 19 of 22 <br /> P 0 BOX 6245 <br /> Stockton, CA 95206 <br /> Volatile Organic Compounds by EPA Method 8260E-Quality Control <br /> Precision Enviro-Tech <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result °/oREC Limits RPD Limit Notes <br /> Batch AL52105-Volattles <br /> Reference(AL52105-SRMI) Prepared&Attalyzed 21-Dec-05 <br /> tcrt Butyl Acohol(TBA) 104 500 ug/] 100 104 75-120 <br /> Methyl tett butyl Ether(MtBE) 400 0 500 400 100 75-120 <br /> Dusopropyl Ether(DIPE) 428 0 500 400 107 75-120 <br /> Ethyl tet Butyl Ether(ETBE) 428 0 500 400 107 75 120 <br /> tert Amyl Methyl Ether(TAME) 428 0 500 400 107 75 120 <br /> 1 2-Dtbromoethane(EDB) 396 0 500 400 99 75 120 <br /> 1,2-Dichloroethane 432 0 500 400 ]OR 75 120 <br /> Benzene 413 0 500 400 103 75 120 <br /> Ethylbenzene 396 050`0 400 99 75 120 <br /> Toluene 195 0 500 400 99 75-120 <br /> wyp-Xylene 393 0 500 400 98 75-120 <br /> lene 397 0 500 400 99 75-120 <br /> mg1L-melligmms per Luer-ppm DLR=Detecnon Ltmlt far Purpose ofReportmg <br /> ug/L-micrograms per Luer-ppb Pseepnowl sample mainces ar interferences may <br /> result in higher detection limits <br /> RESPECTFULLY SUBMITTED, <br /> I <br /> Jonathan LeSf pratory Director <br /> I <br /> 7743 N West Lane Suite B2 Stockton CA 95210 intone (209) 477-8105 Fax (209) 4'7-8148 � <br />