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` PRECISION <br /> EAWMO-TECH <br /> Analytical Laboratory CERTIFICATE OF ANALYSIS <br /> mr Monday,January 10,2005 <br /> ' I <br /> Attention Jack Bishop <br /> California Tank Lines Report Page 18of22 <br /> P 0 BOX 6245 <br /> Stockton,CA 95206 <br /> I Volatile Organic Compounds by EPA Method 8260B-Quality Control <br /> Precision Enviro-Tech <br /> Repomn8 Spike Source %REC RPD <br /> Analyte Result Limn Units Level Result %REC Limits RPD Limit Notes <br /> I <br /> Batch AA50304-Volatiles <br /> Blank(AA50304-BLK1) Prepared 23-Dec-04 Analyzed 23-Dec-05 <br /> tart-Butyl Acohol(TBA) ND 500 No <br /> Methyl tert-butyl Ether(MtBf) ND 0 500 <br /> Dusopropyl Ether(DIPE) ND 0 500 " <br /> Ethyl tort-Butyl Ether(ETBE) ND 0 500 " <br /> ten Amyl Mdhyl Ether(TAME) ND 0 500 <br /> 12 Dibromoedme(EDB) ND 0 500 <br /> l,2-Dtchloroethane ND 0 500 " <br /> 1 Be� ND 0 500 „ <br /> Ethylbenzene ND 0 500 <br /> Toluene ND 0 500 <br /> m""Xylene ND 0 500 " <br /> Wane ND 0 500 " <br /> LCS(AA50304-BSI) Prepared 23-Dec-04 Analyzed 23-Dec-05 <br /> Cert-Butyl Acohoi(TBA) 208 500 ugll 200 104 75-122 <br /> Methyl Cert-butyl Ether(MtBE) 427 0 500 400 107 75 122 <br /> Dusopropyl Ether(DIPE) 422 0 500 400 106 75-122 <br /> Ethyl tert-Butyl Ether(ETBE) 432 0 500 400 108 75-122 <br /> ten Amyl Methyl Ether(TAME) 419 0 500 400 105 75-122 <br /> 12 Dibromoeffime(EDB) 389 0 500 400 97 75-122 <br /> 1,2-Dichloraethime 410 0 500 400 102 75-122 <br /> Benzene 382 0 500 400 % 75-122 <br /> Ethylbeawne 385 0 500 400 % 75-122 <br /> Toluene 391 0 500 400 95 75 122 <br /> in p-Xylene 763 0 500 900 95 75-122 <br /> o-Xylene 391 0 500 400 95 75-122 <br /> Mattel Spike(AA50304-MSI) Source 4121714-01 Prepared 23-Dec-04 Analyzed 23-Dec-05 <br /> tart Butyl Acohol(FBA) 190 500 119/1 200 ND 95 75-122 <br /> Methyl tart butyl Ether(MtBE) 445 0 500 400 ND 111 75-122 <br /> Dusopropyl Ether(DIPE) 418 0500 400 ND 104 75-122 <br /> Ethyl teat-Butyl Ether(ETBE) 404 0 500 400 ND 101 75 122 <br /> tart Amyl Methyl Ether(TAME) 403 0 500 400 ND 101 75-122 <br /> 1,2 Dibromoodme(EDB) 402 0 500 400 ND 100 75-122 <br /> t mg L-mrllrgrrars per Liter-ppm PLR-Detection Lima forParpme ofRepomng <br /> ug L-murvgrama per firer-ppb Fxcepaonal swaple marnces or inrerferencer may <br /> result in higher detection limits <br /> RESPECTFULLY SUBMITTED, <br /> ki/OLAZ� <br /> Jonathan Le,Laboratory Director <br /> F3,V West Lane Suite B2 Stockton C4 95210 phone (209) 47-8105 Fax (209) 4'1'-8148 <br />