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PRECISION <br /> ENVIRO-TECH <br /> Analytical Laboratory CERTIFICATE OF ANALYSIS <br /> Monday January 10,2005 <br /> Attention Jack Bishop <br /> California Tank Lines Report Page 19 of 22 <br /> P 0 BOX 6245 <br /> Stockton,CA 95206 <br /> Volatile Organic Compounds by EPA Method 8260E-Quality Control <br /> Precision Envlro-Tech <br /> Reporting Spike Source %REC RPD <br /> Analytc Result Limit Units Level Result °/nREC Limits RPD Limit Notes <br /> Batch AA50304-Volatiles <br /> Matrix Spike(AA50304-MSI) Source 4121714-01 Prepared 23-Dec-04 Analyzed 23-Dec-05 <br /> 1,2 Dichloroethane 420 0 500 Ujo 400 ND 105 1 75-122 <br /> Benzene 42 l 0 500 400 ND 105 75 122 <br /> Ethylhenzene 429 0 500 400 ND 107 75-122 <br /> Toluene 419 0 500 400 ND 104 75 122 <br /> nip-Xylene 861 0 500 n 900 ND 108 75-122 <br /> o-Xylene 409 0 500 400 ND 102 75-122 <br /> Matrix Spike Dup(AA50304-MSD1) Source 4121714-01 Prepared 23-Dec-04 Analyzed 24-Dec-05 <br /> tort-Butyl Acohol(TBA) 192 500 u94 200 ND 96 75-122 1 15 <br /> Methyl tert-butyl Ether(MtBE) 436 0 500 400 ND 109 75 122 2 15 <br /> Dusapropyl Ether(DIPE) 419 0 500 400 ND 105 75 122 02 is <br /> yl tett-Butyl Ether(ETRE) 423 0 500 M 400 ND 106 75 122 5 i5 <br /> Atayl Methyl Ether(TAME) 403 0 500 400 ND 101 75 122 0 15 <br /> 1,2-Dibromoetti ne(EDB) 399 0 500 400 ND 100 75 122 1 15 <br /> 12 Dictiloroedme 420 0 500 400 ND 105 75-122 0 15 <br /> Benzene 400 0 500 400 ND 100 75-122 5 15 <br /> Ethylbenzene 405 0 500 400 ND 101 75-122 6 15 <br /> Toluene 404 0 500 400 ND 101 75-122 3 15 <br /> in p-Xylene 800 0 500 800 ND 100 75-122 7 15 <br /> o-Xylene 401 0 500 400 ND 100 75 122 2 15 <br /> mgL-milligrams per Liter-pan DLR-Defection Lumtfor Purpose of Reporting <br /> ug L-micrograms per Luer-ppb Ex eptnmal sample mamm or inrerferences may <br /> result in higher detection hmits. <br /> RESPECTFULLY SUBMITTED, <br /> 118(:�5/Ot'.r� <br /> Jonathan Le,Laboratory Director <br /> -743.V West Lune Suite B2 Stockton C4 95210 phone (209) 47"-8105 Fax (209) 477-8148 <br />