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0 0 <br />Blank Spike/Blank Spike Duplicate Summary Page I of 3 <br />Job Number: C17729 <br />Account: GEAICAO Giles Engineering Associates, Inc. <br />Project: 239 West 11th Street - Tracy, CA <br />Sample <br />File ID <br />DF <br />Analyzed <br />By <br />Prep Date <br />Prep Batch <br />Analytical Batch <br />VM861-BS <br />M27127.1) <br />1 <br />09/02/11 <br />XB <br />n/a <br />n/a <br />VM861 <br />VM861-BSD <br />M27128.1) <br />1 <br />09/02/11 <br />XB <br />n/a <br />n/a <br />VM861 <br />The QC reported here applies to the following samples: Method: SW846 8260B <br />C17729-1, C17729-2, C17729-3, C17729-4, C17729-5 <br />I 1 <br />v <br />me 37 of 50 <br />' w ACCUTEST. <br />CM29 <br />Spike <br />BSP <br />BSP <br />BSD <br />BSD <br />Limits <br />CAS No. <br />Compound <br />ug/kg <br />ug/kg <br />% <br />ug/kg <br />% <br />RPD <br />Rec/RPD <br />67-64-1 <br />Acetone <br />160 <br />193 <br />121 <br />208 <br />130 <br />7 <br />60-130/30 <br />71-43-2 <br />Benzene <br />40 <br />43.1 <br />108 <br />51.6 <br />129 <br />18 <br />60-130/30 <br />108-86-1 <br />Bromobenzene <br />40 <br />41.1 <br />103 <br />49.6 <br />124 <br />19 <br />60-130/30 <br />74-97-5 <br />Bromochloromethane <br />40 <br />42.3 <br />106 <br />51.5 <br />129 <br />20 <br />60-130/30 <br />75-27-4 <br />Bromodichloromethane <br />40 <br />41.9 <br />105 <br />49.6 <br />124 <br />17 <br />60-130/30 <br />75-25-2 <br />Bromoform <br />40 <br />40.3 <br />101 <br />47.3 <br />118 <br />16 <br />60-130/30 <br />104-51-8 <br />n-Butylbenzene <br />40 <br />43.1 <br />108 <br />52.1 <br />130 <br />19 <br />60-130/30 <br />135-98-8 <br />sec-Butylbenzene <br />40 <br />43.0 <br />108 <br />52.1 <br />130 <br />19 <br />60-130/30 <br />98-06-6 <br />terl-Butylbenzene <br />40 <br />42.6 <br />107 <br />51.4 <br />129 <br />19 <br />60-130/30 <br />108-90-7 <br />Chlorobenzene <br />40 <br />41.2 <br />103 <br />51.2 <br />128 <br />22 <br />60-130/30 <br />75-00-3 <br />Chloroethane <br />40 <br />44.3 <br />111 <br />52.0 <br />130 <br />16 <br />60-130/30 <br />67-66-3 <br />Chloroform <br />40 <br />42.0 <br />105 <br />50.4 <br />126 <br />18 <br />60-130/30 <br />95-49-8 <br />o-Chlorotoluene <br />40 <br />42.4 <br />106 <br />52.8 <br />132* a <br />22 <br />60-130/30 <br />106-43-4 <br />p-Chlorotoluene <br />40 <br />42.5 <br />106 <br />49.7 <br />124 <br />16 <br />60-130/30 <br />56-23-5 <br />Carbon tetrachloride <br />40 <br />39.0 <br />98 <br />47.2 <br />118 <br />19 <br />60-130/30 <br />75-34-3 <br />1,1-Dichloroethane <br />40 <br />43.4 <br />109 <br />52.2 <br />131* a <br />18 <br />60-130/30 <br />75-35-4 <br />1,1-Dichloroethylene <br />40 <br />45.5 <br />114 <br />55.5 <br />139* a <br />20 <br />60-130/30 <br />563-58-6 <br />1,1-Dichloropropene <br />40 <br />42.7 <br />107 <br />51.5 <br />129 <br />19 <br />60-130/30 <br />96-12-8 <br />1,2-Dibromo-3-chloropropane <br />40 <br />46.5 <br />116 <br />54.1 <br />135* a <br />15 <br />60-130/30 <br />106-93-4 <br />1,2-Dibromoethane <br />40 <br />41.6 <br />104 <br />49.8 <br />125 <br />18 <br />60-130/30 <br />107-06-2 <br />1,2-Dichloroethane <br />40 <br />40.5 <br />101 <br />47.4 <br />119 <br />16 <br />60-130/30 <br />78-87-5 <br />1,2-Dichloropropane <br />40 <br />42.6 <br />107 <br />51.3 <br />128 <br />19 <br />60-130/30 <br />142-28-9 <br />1,3-Dichloropropane <br />40 <br />41.7 <br />104 <br />50.5 <br />126 <br />19 <br />60-130/30 <br />108-20-3 <br />Di -Isopropyl ether <br />40 <br />44.4 <br />111 <br />52.8 <br />132* a <br />17 <br />60-130/30 <br />594-20-7 <br />2,2-Dichloropropane <br />40 <br />42.0 <br />105 <br />51.5 <br />129 <br />20 <br />60-130/30 <br />124-48-1 <br />Dibromochloromethane <br />40 <br />39.6 <br />99 <br />48.3 <br />121 <br />20 <br />60-130/30 <br />75-71-8 <br />Dichlorodifluoromethane <br />40 <br />31.9 <br />80 <br />37.6 <br />94 <br />16 <br />60-130/30 <br />156-59-2 <br />cis-1,2-Dichloroethylene <br />40 <br />43.2 <br />108 <br />52.2 <br />131* a <br />19 <br />60-130/30 <br />10061-01-5 <br />cis-1,3-Dichloropropene <br />40 <br />43.2 <br />108 <br />50.7 <br />127 <br />16 <br />60-130/30 <br />541-73-1 <br />m -Dichlorobenzene <br />40 <br />41.2 <br />103 <br />49.4 <br />124 <br />18 <br />60-130/30 <br />95-50-1 <br />o -Dichlorobenzene <br />40 <br />41.2 <br />103 <br />49.8 <br />125 <br />19 <br />60-130/30 <br />106-46-7 <br />p -Dichlorobenzene <br />40 <br />41.2 <br />103 <br />49.7 <br />124 <br />19 <br />60-130/30 <br />156-60-5 <br />trans-1,2-Dichloroethylene <br />40 <br />43.9 <br />110 <br />53.4 <br />134* a <br />20 <br />60-130/30 <br />10061-02-6 <br />trans-1,3-Dichloropropene <br />40 <br />41.2 <br />103 <br />50.4 <br />126 <br />20 <br />60-130/30 <br />100-41-4 <br />Ethylbenzene <br />40 <br />41.5 <br />104 <br />51.8 <br />130 <br />22 <br />60-130/30 <br />637-92-3 <br />Ethyl tert-Butyl Ether <br />40 <br />43.9 <br />110 <br />52.2 <br />131* a <br />17 <br />60-130/30 <br />I 1 <br />v <br />me 37 of 50 <br />' w ACCUTEST. <br />CM29 <br />