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1 <br />I <br />1 <br />1 <br />0 9 <br />Blank Spike/Blank Spike Duplicate Summary Page 2 of 3 <br />Job Number: C17729 <br />Account: GEAICAO Giles Engineering Associates, Inc. <br />Project: 239 West 11th Street - Tracy, CA <br />Sample <br />File ID <br />DF <br />Analyzed <br />By <br />Prep Date <br />Prep Batch <br />Analytical Batch <br />VM861-BS <br />M27127.1) <br />1 <br />09/02/11 <br />XB <br />n/a <br />n/a <br />VM861 <br />VM861-BSD <br />M27128.D <br />1 <br />09/02/11 <br />XB <br />n/a <br />n/a <br />VM861 <br />The QC reported here applies to the following samples: Method: SW846 8260B <br />C17729-1, C17729-2, C17729-3, C17729-4, C17729-5 <br />4; <br />J <br />ME 38 of 50 <br />■ ACGUTEST. <br />017729 `..... I- - <br />Spike <br />BSP <br />BSP <br />BSD <br />BSD <br />Limits <br />CAS No. <br />Compound <br />ug/kg <br />ug/kg <br />% <br />ug/kg <br />% <br />RPD <br />Rec/RPD <br />591-78-6 <br />2-Hexanone <br />160 <br />177 <br />111 <br />197 <br />123 <br />11 <br />60-130/30 <br />87-68-3 <br />Hexachlorobutadiene <br />40 <br />39.5 <br />99 <br />47.7 <br />119 <br />19 <br />60-130/30 <br />98-82-8 <br />Isopropylbenzene <br />40 <br />41.0 <br />103 <br />51.5 <br />129 <br />23 <br />60-130/30 <br />99-87-6 <br />p-Isopropyltoluene <br />40 <br />42.4 <br />106 <br />51.5 <br />129 <br />19 <br />60-130/30 <br />108-10-1 <br />4-Methyl-2-pentanone <br />160 <br />179 <br />112 <br />196 <br />123 <br />9 <br />60-130/30 <br />74-83-9 <br />Methyl bromide <br />40 <br />42.3 <br />106 <br />50.5 <br />126 <br />18 <br />60-130/30 <br />74-87-3 <br />Methyl chloride <br />40 <br />35.2 <br />88 <br />45.8 <br />115 <br />26 <br />60-130/30 <br />74-95-3 <br />Methylene bromide <br />40 <br />41.5 <br />104 <br />47.9 <br />120 <br />14 <br />60-130/30 <br />75-09-2 <br />Methylene chloride <br />40 <br />39.7 <br />99 <br />48.0 <br />120 <br />19 <br />60-130/30 <br />78-93-3 <br />Methyl ethyl ketone <br />160 <br />195 <br />122 <br />210 <br />131* a <br />7 <br />60-130/30 <br />1634-04-4 <br />Methyl Tert Butyl Ether <br />40 <br />44.6 <br />112 <br />52.1 <br />130 <br />16 <br />60-130/30 <br />91-20-3 <br />Naphthalene <br />40 <br />45.7 <br />114 <br />51.8 <br />130 <br />13 <br />60-130/30 <br />103-65-1 <br />n-Propylbenzene <br />40 <br />43.9 <br />110 <br />53.3 <br />133* a <br />19 <br />60-130/30 <br />100-42-5 <br />Styrene <br />40 <br />41.3 <br />103 <br />50.9 <br />127 <br />21 <br />60-130/30 <br />994-05-8 <br />Tert-Amyl Methyl Ether <br />40 <br />43.9 <br />110 <br />51.6 <br />129 <br />16 <br />60-130/30 <br />75-65-0 <br />Tert Butyl Alcohol <br />200 <br />256 <br />128 <br />272 <br />136* a <br />6 <br />60-130/30 <br />630-20-6 <br />1,1,1,2 -Tetrachloroethane <br />40 <br />39.2 <br />98 <br />49.6 <br />124 <br />23 <br />60-130/30 <br />71-55-6 <br />1,1,1 -Trichloroethane <br />40 <br />41.9 <br />105 <br />50.6 <br />127 <br />19 <br />60-130/30 <br />79-34-5 <br />1,1,2,2 -Tetrachloroethane <br />40 <br />45.6 <br />114 <br />52.1 <br />130 <br />13 <br />60-130/30 <br />79-00-5 <br />1,1,2 -Trichloroethane <br />40 <br />40.8 <br />102 <br />49.8 <br />125 <br />20 <br />60-130/30 <br />87-61-6 <br />1,2,3-Trichlorobenzene <br />40 <br />41.7 <br />104 <br />49.1 <br />123 <br />16 <br />60-130/30 <br />96-18-4 <br />1,2,3-Trichloropropane <br />40 <br />43.3 <br />108 <br />50.1 <br />125 <br />15 <br />60-130/30 <br />120-82-1 <br />1,2,4-Trichlorobenzene <br />40 <br />41.4 <br />104 <br />49.7 <br />124 <br />18 <br />60-130/30 <br />95-63-6 <br />1,2,4-Trimethylbenzene <br />40 <br />42.4 <br />106 <br />51.0 <br />128 <br />18 <br />60-130/30 <br />108-67-8 <br />1, 3,5 -Trimethylbenzene <br />40 <br />43.1 <br />108 <br />52.1 <br />130 <br />19 <br />60-130/30 <br />127-18-4 <br />Tetrachloroethylene <br />40 <br />39.7 <br />99 <br />49.8 <br />125 <br />23 <br />60-130/30 <br />108-88-3 <br />Toluene <br />40 <br />41.7 <br />104 <br />52.0 <br />130 <br />22 <br />60-130/30 <br />79-01-6 <br />Trichloroethylene <br />40 <br />42.2 <br />106 <br />50.5 <br />126 <br />18 <br />60-130/30 <br />75-69-4 <br />Trichlorofluoromethane <br />40 <br />39.6 <br />99 <br />46.7 <br />117 <br />16 <br />60-130/30 <br />75-01-4 <br />Vinyl chloride <br />40 <br />39.7 <br />99 <br />48.0 <br />120 <br />19 <br />60-130/30 <br />1330-20-7 <br />Xylene (total) <br />120 <br />122 <br />102 <br />152 <br />127 <br />22 <br />60-130/30 <br />CAS No. <br />Surrogate Recoveries <br />BSP <br />BSD <br />Limits <br />1868-53-7 <br />Dibromofluoromethane <br />96% <br />95% <br />60-130% <br />4; <br />J <br />ME 38 of 50 <br />■ ACGUTEST. <br />017729 `..... I- - <br />