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Ms.Lori Duncan <br /> Page 2 of 3 pages <br /> Stockpile and Excavation Sample Collection <br /> Ground Zero collected a 3:1 composite of the stockpile and two (2) floor samples from the <br /> excavation. Soil samples were collected in brass tubes, sealed with Teflon® sheets and plastic caps, <br /> uniquely labeled, temporarily stored on ice in an ice chest cooled to approximately 4°C, and were <br /> delivered under chain of custody protocol to Argon Laboratories of Ceres, California(Argon). <br /> Soil samples were analyzed for the following: <br /> • TPHg, TPHd, and TPHmo by EPA method 8015M <br /> • Full list of VOCs by EPA method 8260B <br /> • LUFT 5 Metals by EPA method 6010B <br /> • pH by SM4500-H+B <br /> Analytical Results <br /> The excavation floor sample and stockpile results are summarized as follows: <br /> Floor 1 <br /> • pH was 6.7 pH units <br /> • LUFT metals: Cadmium <1.0 milligrams per kilogram (mg/Kg), Chromium 9.8 mg/Kg, Lead <br /> 27 mg/Kg,Nickel 6.1 mg/Kg, and Zinc 64 mg/Kg. <br /> • No other analyzed constituent was reported above laboratory detection limits. <br /> Floor 2 <br /> • pH was 6.5 pH units <br /> • LUFT metals: Cadmium <1.0 milligrams per kilogram (mg/Kg), Chromium 8.8 mg/Kg, Lead <br /> 11 mg/Kg,Nickel 7.8 mg/Kg, and Zinc 46 mg/Kg. <br /> • No other analyzed constituent was reported above laboratory detection limits. <br /> Stoc ile <br /> • pH was 6.6 pH units <br /> • LUFT metals: Cadmium <1.0 milligrams per kilogram (mg/Kg), Chromium 9.0 mg/Kg, Lead <br /> 92 mg/Kg,Nickel 4.4 mg/Kg, and Zinc 440 mg/Kg. <br /> • No other analyzed constituent was reported above laboratory detection limits. <br /> Upon review of the analytical data Ground Zero requested that Argon ran a Soluble Threshold <br /> Limit Concentration (STLC) analysis for lead in the stockpile sample based on California Code <br /> of Regulations Title 22 Limits for Hazardous Waste (CCR 22261.24). The STLC result for lead <br /> in the stockpile sample was 4.3 milligrams per liter (mg/L) and below the threshold of 5.0 mg/L. <br /> The laboratory analytical results are included in Attachment B. <br />