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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 14 1 http//wwwmccampbellcorn E-mail main@mccampbell corn <br /> GEOSOLV, LLC Client Project ID Nunan/Jemigan Date Sampled 03/10/01 <br /> 643 Oregon Street Date Received 03/10/01 <br />' Sonoma,CA 95476 Client Contact Frank Goldman Date Extracted 03/13/01 <br /> Client P O Date Analyzed 03/13/01 <br /> Volatile Organics By GC/MS ' <br /> EPA method 8260 <br /> Lab ID 62406 <br /> Client ID MW-1 <br /> Matnx W <br /> Reporting Limit Reporting Lint <br /> Compound Concentration* W S Compound Concentration* W S <br /> Acetone(b) ND 30 25 trans-f,3-Dichloropropene ND 10 50 <br /> Benzene ND 1 0 50 Ethylene dibromide ND 10 5 0 <br />' Bromobenzene ND 10 5 0 Ethylbenzene ND 10 5 0 <br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 10 5 0 lodomethane ND 10 5 0 <br /> Bromoform ND 10 50 Isopropyibenzene ND to 5 0 <br />' Bromomethane ND 10 50 p-Isopropyl toluene ND 10 50 <br /> n-Butyl benzene ND 1 0 50 1 Methyl butyl ketone ND 10 50 <br /> sec-Butyl benzene ND 10 50 Methylene Chloride` ND 10 50 <br /> tert-Butyl benzene ND 10 5 0 Methyl ethyl ketone ND 2 0 10 <br /> Carbon Disulfide ND 10 5 0 Methyl isobutyl ketones ND 10 5 0 <br /> Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyl Ether(M I BE) 10 5 0 <br /> Chlorobenzene ND to 50 Naphthalene ND 50 50 <br /> Chloroethane ND 10 5 0 n-Propyl benzene ND 10 50 <br />' 2-Chloroethyl Vinyl Ether") ND 1 0 5 0 Styrene ND 1 0 1 50 <br /> Chloroform ND 10 5 0 1,1,1,2-Tetrachloroethane ND 10 5 0 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 10 5 0 <br /> 2-Chlorotoluene ND 10 50 Tetrachloroethene ND 10 50 <br />' 4-Chlorotoluene ND 1 0 5 0 Toluene ND 10 50 <br /> Dibromochloromethane ND 1 0 50 l,2,3-Trichlorobenzene ND 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Tnchlorobenzene ND 50 25 <br /> Dibromomethane ND 10 5 0 1,1,1-Tnchloroethane ND 10 50 <br />' 1,2-Dich1orobenzene ND 10 50 1,1,2-Trichloroethane ND 10 5 0 <br /> 1,3-Dichlorobenzene ND 1 0 5 0 Trichloroethene ND 10 5 0 <br /> 1 4-Dichlorobenzene ND 1 0 5 0 Tnchlorofluoromethane ND 10 5 0 <br /> Dichlorodifluoromethane ND 10 5 0 1,2,3-Tnehloropropane ND to 5 0 <br />' l,1-Dichloroethane ND 10 50 1,2,4-Trinxthylbenzene ND 10 5 0 <br /> 1,2-Dichloroethane ND 10 5 0 1,3,5-Tnmethylbenzene ND 10 50 <br /> I,l-Dichloroethene ND 1 0 5 0 Vinyl Acetate"F- ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 1 0 50 Vinyl Chloride " ND 10 5 0 <br />' <br /> trans-l,2-Dichloroethene ND 10 5 0 Xylenes,total ND 10 5 0 <br /> 1,2-Dichloropropane ND 10 50 Comments <br /> 1,3-Dichloropropane ND 1 0 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 5 0 Dibromotluoromethane 114 <br />' 1,1-Dichloropropene ND 10 5 0 Toluene-d8 100 <br /> cis-1,3-Dichloropropene ND 10 50 4-Bromofluorobenzene 107 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br />' ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone, (e) dichloromethane (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone (h)lighter than water immiscible sheen is present, (1) liquid sample that contains greater than --5 vol % <br /> sediment, (t) sample diluted due to high organic content (k) ethenylbenzene (1) methylbenzene (m) acetic acid ethenyl ester (n) <br /> chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hanulton,Lab Director <br />