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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> MCCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell coin E-mail main@mccampbell coin <br /> I, GEOSOLV,LL.0 Client Project 1D Nunan/Jernigan Date Sampled 03/10/01 <br /> 643 Oregon Street Date Received 03/10/01 <br /> Sonoma, CA 95476 Client Contact Frank Goldman Date Extracted 03/13/01 <br /> 1 Client P O Date Analyzed 03/13/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> 1 Lab ID 62407 <br /> Client 1D MW-2 <br /> Matrix W <br /> Compound Concentration* Reporting Limit Compound Concentration* Reporting Limit <br />' W S W S <br /> Acetone(5) ND 50 25 trans-1,3-Dichloropropene ND 10 50 <br /> Benzene ND 10 50 Ethylene dibromide ND 10 50 <br /> 1 Bromobenzene ND 10 50 Ethylbenzene ND 10 50 <br /> Bromochloromethane ND 10 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 10 50 Iodomethane ND 10 50 <br /> Bromoform ND 10 50 Isopropylbenzene ND l 0 50 <br /> 1 Bromomethane ND 1 0 50 p-lsopropyl toluene ND 10 50 <br /> n-Butyl benzene ND 1 0 50 Methyl butyl ketone ND 10 50 <br /> sec-Butyl benzene ND 10 50 Methylene Chlonde` ND 10 50 <br /> tert-Butyl benzene ND 1 0 50 Methyl ethyl ketone ND 20 10 <br /> Carbon Disulfide ND 10 50 Methyl isobutyl ketones ND 10 50 <br /> Carbon Tetrachloride ND 1 0 50 Methyl tert-Butyi Ether(MTBE) 10 50 <br /> Chlorobenzene ND 10 50 Naphthalene ND 50 so <br /> Chloroethane ND 10 50 n-Propyl benzene ND 1 0 50 <br />' 2-Chloroethyl Vinyl Ethe ND 10 50 Styrene ND 1 0 50 <br /> Chloroform ND 10 50 1,1,1,2-Tetrachloroethane ND 10 50 <br /> Chloromethane ND 10 50 1,1,2,2-Tetrachloroethane ND 10 50 <br /> 2-Chlorotoluene ND 10 50 Tetrachloroethene ND 16 50 <br />' 4-Chlorotoluene ND 10 50 Toluene 59 10 50 <br /> Dibromochlommethane ND 10 50 1,2,3-Trichlorobenzene ND 50 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 10 1,2,4-Trichtorobenzene ND 50 25 <br /> DibrOmOmethane ND 10 50 1,10-Trichloroethane ND 10 50 <br />' 1,2-Dichlorobenzene ND 1 0 50 1,1,2-Trichloroethane ND 1 0 50 <br /> 1 3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 1 0 50 <br /> 1,4-Dichlorobenzene ND 1 0 5 0 Trichlorofluaromethane ND 1 0 5 0 <br /> Dichlorodifluoromethane ND 10 5 0 1,2,3-Tnchloropropane ND 10 50 <br />' 1,1-Dichloroethane ND 10 5 0 1,2,4-Tnmethylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 10 5 0 1,3,5-Tnmethylbenzene ND 10 50 <br /> 1,1-Dichloroethene ND 10 5 0 Vinyl Acetate " ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 1 0 5 0 Vinyl Chloride ° ND 10 5 0 <br /> trans-1,2-Dichloroethene ND 1 0 5 0 Xylenes,total ND 1 0 i 5 0 <br /> 1,2-Dichloropropane ND 10 1 50 Comments <br /> 1,3-Diehl oropropane ND 10 50 Surrogate Recoveries(%) <br /> 2,2-Dicbloropropane ND 1 0 5 0 Dibromefluoromethane 114 <br />' I,I-Dichloropropene ND 10 50 Toluene-d8 96 <br /> cis-1,3-Dichloropropene ND 10 1 50 4-Bromofluorobenzene 104 <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit NIA means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane (f) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h)lighter than water immiscible sheen as present, (i) liquid sample that contains greater than --5 vol <br />' sediment, ') sample diluted due to high organic content (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester (n) <br /> chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />