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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> 4 1 WCA.MPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> 11th//www mccampbell com E-mail main@mccampbell com <br /> 1 GEOSOLV,LLC Client Project ID Nunan/Jemigan Date Sampled 02120-03/0 1/01 <br /> 643 Oregon Street Date Received 03/01/01 <br /> Sonoma,CA 95476 Client Contact Frank Goldman Date Extracted 03/05/01 <br /> Client P O Date Analyzed 03/05-03/08/01 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab ID 61491 <br /> Client ID MW-1 23 -24 <br /> Matrix S <br /> Reporting Limit Reporting Lima <br /> jAcetone <br /> pound Concentration* W S Compound Concentration* W S <br /> mf ND<35 50 25 jEthylbenzene <br /> s-],3-Dichloropropene ND 10 50 <br /> zene ND 10 50 ylene dibromide ND 10 50 <br /> mobenzene ND 1 0 5 0 ND 1 0 5 0 <br /> Bromochloromethane ND 1 0 50 Hexachlorobutadiene ND 50 25 <br /> Bromodichloromethane ND 1 0 1 5 0 lodomethane ND 10 50 <br /> Bromofonn ND 10 50 Isopropylbenzene ND 10 5 0 <br /> Bromomethane ND 10 50 p-Isopropyl toluene ND 10 5 0 <br /> n-Butyl benzene ND 1 0 5 0 Methyl butyl ketone ND 1 0 50 <br /> sec-Butyl benzene ND 1 0 50 Methylene Chlonde` ND 10 50 <br /> tent-Butyl benzene i ND 10 5 0kmlib <br /> l ethyl ketone ND 20 10 <br /> Carbon Disulfide ND t 0 50 l isobutyl ketone8) ND —10 50 <br /> Carbon Tetrachloride ND 10 5 0 l Cert Butyl Ether(MTBE) -- 10 50 <br /> 10 Chlorobenzene ND 1 0 5 0 halene ND 5 0 50 <br /> Chloroethane ND ] 0 50 pyl benzene ND 10 50 <br /> 2-Chloroethyl Vinyl Ethe ND 1 0 5 0 e ND t 0 5 0 <br /> Chloroform ND ] 0 5 0 2-Tetrachloroethane ND l 0 5 0 <br /> Chloromethane ND 1 0 5 0 2-Tetrachloroethane ND 10 5 0 <br /> 2-Chlorotoluene ND 1 0 50 hloroethene ND 10 50 <br /> 4-Chlorotoluene ND 10 5 0 ne38 1 0 5 0 <br /> Dibromochloromethane ND 1 0 5 0 Tnchlorobenzene ND 5 0 25 <br /> 1,2-Dibromo-3-chloropropane ND 20 l0 , , Trichlorobenzene ND 50 25 <br /> Dibromometbane ND 1 0 5 0 1,1,1-Tnchloroethane ND 10 5 0 <br /> 1,2-Dichlorobenzene ND 10 50 1,1,2-Tnchloroethane ND 10 50 <br />' 1,3-Dichlorobenzene ND 1 0 50 Trichloroethene ND 10 50 <br /> 1,4-Dtchlorobenzene ND 1 0 50 Tneblarofluoromethane ND 1 0 50 <br /> Di chlorodiIIuoromethane ND 1 0 50 1,2,3-Tnchtoropropane ND 10 50 <br /> 1 1-Dichloroethane ND 1 0 5 0 1,2,4-Trimathylbenzene ND 10 50 <br /> 1,2-Dichloroethane ND 1 0 5 0 1,3,5-Trinvthylbenzene ND 10 5 0 <br /> 1,1-Dich1oroethene ND 1 0 5 0 Vinyl Acetate m ND 5 0 25 <br /> cis-1,2-Dichloroethene ND 10 5 0 Vinyl Chloride " ND 1 10 5 0 <br /> trans-l,2-Dichloroethene ND 10 5 0 Xylenes,total ND 10 50 <br /> 1,2-Dichloropropane ND 10 5 0 Comments <br /> 1,3-Dtchloropropane ND 1 0 5 0 Surrogate Recoveries(%) <br /> 2,2-Dichloropropane ND 1 0 5 0 Dibromotluoromethane 102 <br /> 111-Dichlo1opropene ND 1 0 5 0 TolueneA8 106 <br /> cis-1,3-Dichloropropene ND 1 4 50 4-Bramofluorobenzene 94 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> ND means not detected above the reporting hrmt,N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone (c) (2-chloroethoxy) ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacetone,(h) lighter than water immiscible sheen is present, (i)liquid sample that contains greater than --5 vol % <br /> sediment 0) sample diluted due to high organic content, (k) ethenylbenzene, (1) methylbenzene, (m) acetic acid ethenyl ester, (n) <br /> chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hairulton,Lab Director <br />